N^G-carbobenzoxy-4-guanidinobutanal

Base Information

Chemical Name:N^G-carbobenzoxy-4-guanidinobutanal
CAS No.:212328-82-0
Molecular Formula:C₁₃H₁₇N₃O₃
Molecular Weight:263.296
Hs Code.:

N<sup>G</sup>-carbobenzoxy-4-guanidinobutanal

Synonyms:N^G-carbobenzoxy-4-guanidinobutanal

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Chemical Property of N^G-carbobenzoxy-4-guanidinobutanal

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Technology Process of N^G-carbobenzoxy-4-guanidinobutanal

There total 4 articles about N^G-carbobenzoxy-4-guanidinobutanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 212328-81-9
methyl N^G-carbobenzoxy-4-guanidinobutanoate

: 212328-82-0
N^G-carbobenzoxy-4-guanidinobutanal

Guidance literature:: With diisobutylaluminium hydride; In diethylene glycol dimethyl ether; at -30 ℃; for 2h;
DOI:10.1021/jo980070c

Reference yield:

: 463-00-3
4-guanidinobutyric acid

: 212328-82-0
N^G-carbobenzoxy-4-guanidinobutanal

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) SOCl₂ / 1.) room temperature, 18 h, 2.) -78 deg C to room temperature, 3 h

2: 65 percent / NaOMe / methanol / 1.) 0 deg Cm 2 h, 2.) room temperature, 18 h

3: 69 percent / DIBAL / bis-(2-methoxy-ethyl) ether / 2 h / -30 °C

With thionyl chloride; sodium methylate; diisobutylaluminium hydride; In methanol; diethylene glycol dimethyl ether;
DOI:10.1021/jo980070c

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 212328-82-0
N^G-carbobenzoxy-4-guanidinobutanal

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / NaOMe / methanol / 1.) 0 deg Cm 2 h, 2.) room temperature, 18 h

2: 69 percent / DIBAL / bis-(2-methoxy-ethyl) ether / 2 h / -30 °C

With sodium methylate; diisobutylaluminium hydride; In methanol; diethylene glycol dimethyl ether;
DOI:10.1021/jo980070c