disodium 3α-acetoxy-12α-hydroxy-7-oxo-5β-cholan-24-oate 12-sulfate

Base Information

• Chemical Name: disodium 3α-acetoxy-12α-hydroxy-7-oxo-5β-cholan-24-oate 12-sulfate
• CAS No.: 77499-35-5
• Molecular Formula: C₂₆H₃₈O₉S*2Na
• Molecular Weight: 572.628

Synonyms:disodium 3α-acetoxy-12α-hydroxy-7-oxo-5β-cholan-24-oate 12-sulfate

Chemical Property of disodium 3α-acetoxy-12α-hydroxy-7-oxo-5β-cholan-24-oate 12-sulfate

Chemical Property:

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Technology Process of disodium 3α-acetoxy-12α-hydroxy-7-oxo-5β-cholan-24-oate 12-sulfate

There total 1 articles about disodium 3α-acetoxy-12α-hydroxy-7-oxo-5β-cholan-24-oate 12-sulfate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

7-ketodeoxycholic acid (911-40-0) → disodium 3α-acetoxy-12α-hydroxy-7-oxo-5β-cholan-24-oate 12-sulfate (77499-35-5)

Guidance literature:

Multi-step reaction with 4 steps

1: 330 mg / pyridine / H₂O; benzene / Ambient temperature

2: 260 mg / chlorosulfonic acid, pyridine / 1 h / 50 °C / ice-cooling (adding)

3: 218 mg / aq. NaOH / methanol

4: 23 mg / pyridine / 4 h / Ambient temperature

With pyridine; chlorosulfonic acid; sodium hydroxide; In methanol; water; benzene;

upstream raw materials:

7-ketodeoxycholic acid

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