(S)-2-(tert-butoxycarbonylamino)-3-(4-hydroxy-3-iodo-5-nitrophenyl)propanoic acid

Base Information

Chemical Name:(S)-2-(tert-butoxycarbonylamino)-3-(4-hydroxy-3-iodo-5-nitrophenyl)propanoic acid
CAS No.:1253795-07-1
Molecular Formula:C₁₄H₁₇IN₂O₇
Molecular Weight:452.203
Hs Code.:

Synonyms:(S)-2-(tert-butoxycarbonylamino)-3-(4-hydroxy-3-iodo-5-nitrophenyl)propanoic acid

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Chemical Property of (S)-2-(tert-butoxycarbonylamino)-3-(4-hydroxy-3-iodo-5-nitrophenyl)propanoic acid

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Technology Process of (S)-2-(tert-butoxycarbonylamino)-3-(4-hydroxy-3-iodo-5-nitrophenyl)propanoic acid

There total 3 articles about (S)-2-(tert-butoxycarbonylamino)-3-(4-hydroxy-3-iodo-5-nitrophenyl)propanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 5575-03-1
(2S)-2-tert-butoxycarbonylamino-3-(4-hydroxy-3-nitro-phenyl)-propionic acid

: 1253795-07-1
(S)-2-(tert-butoxycarbonylamino)-3-(4-hydroxy-3-iodo-5-nitrophenyl)propanoic acid

Guidance literature:: With iodine; silver trifluoroacetate; In chloroform; at 20 ℃; for 2h; Darkness; Inert atmosphere;
DOI:10.1002/chem.201000924

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1253795-07-1
(S)-2-(tert-butoxycarbonylamino)-3-(4-hydroxy-3-iodo-5-nitrophenyl)propanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate / water; acetone

2: sodium hydrogencarbonate; N,N,N-trimethylbenzenemethanaminium dichloroiodate / methanol; dichloromethane

With sodium hydrogencarbonate; N,N,N-trimethylbenzenemethanaminium dichloroiodate; In methanol; dichloromethane; water; acetone;
DOI:10.1021/np200163g

Reference yield:

: 621-44-3
3-nitro-L-tyrosine

: 1253795-07-1
(S)-2-(tert-butoxycarbonylamino)-3-(4-hydroxy-3-iodo-5-nitrophenyl)propanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate / water; acetone

2: sodium hydrogencarbonate; N,N,N-trimethylbenzenemethanaminium dichloroiodate / methanol; dichloromethane

With sodium hydrogencarbonate; N,N,N-trimethylbenzenemethanaminium dichloroiodate; In methanol; dichloromethane; water; acetone;
DOI:10.1021/np200163g