C₁₅H₁₅BrO₂

Base Information

• Chemical Name: C₁₅H₁₅BrO₂
• CAS No.: 1443418-26-5
• Molecular Formula: C₁₅H₁₅BrO₂
• Molecular Weight: 307.187
• Mol file: 1443418-26-5.mol

Synonyms:C₁₅H₁₅BrO₂

Chemical Property of C₁₅H₁₅BrO₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₅H₁₅BrO₂

There total 3 articles about C₁₅H₁₅BrO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

2,5-Dimethylphenol (95-87-4) + 1-Bromo-2-chloro-methoxybenzene (54257-94-2) → C15H15BrO2 (1443418-26-5)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 40 ℃; for 24h; Inert atmosphere;

DOI:10.1002/chem.201301969

Reference yield:

2-hydroxybromobenzene (95-56-7) → C15H15BrO2 (1443418-26-5)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium hydride / N,N-dimethyl-formamide

2: sulfuryl dichloride / dichloromethane

3: potassium carbonate / N,N-dimethyl-formamide

With sulfuryl dichloride; sodium hydride; potassium carbonate; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1002/anie.201207485

Reference yield:

1-bromo-2-[(methylsulfanyl)methoxy]benzene (592508-12-8) → C15H15BrO2 (1443418-26-5)

Guidance literature:

Multi-step reaction with 2 steps

1: sulfuryl dichloride / dichloromethane

2: potassium carbonate / N,N-dimethyl-formamide

With sulfuryl dichloride; potassium carbonate; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1002/anie.201207485

upstream raw materials:

2-hydroxybromobenzene

1-bromo-2-[(methylsulfanyl)methoxy]benzene

2,5-Dimethylphenol

1-Bromo-2-chloro-methoxybenzene