5-(3-((2-(dimethylamino)ethyl)amino)-5-fluorophenyl)pyridine-3,4-diamine

Base Information

• Chemical Name: 5-(3-((2-(dimethylamino)ethyl)amino)-5-fluorophenyl)pyridine-3,4-diamine
• CAS No.: 1467083-68-6
• Molecular Formula: C₁₅H₂₀FN₅
• Molecular Weight: 289.356

Synonyms:5-(3-((2-(dimethylamino)ethyl)amino)-5-fluorophenyl)pyridine-3,4-diamine

Chemical Property of 5-(3-((2-(dimethylamino)ethyl)amino)-5-fluorophenyl)pyridine-3,4-diamine

Chemical Property:

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Technology Process of 5-(3-((2-(dimethylamino)ethyl)amino)-5-fluorophenyl)pyridine-3,4-diamine

There total 6 articles about 5-(3-((2-(dimethylamino)ethyl)amino)-5-fluorophenyl)pyridine-3,4-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.8%

N1-(3-(4-amino-5-nitropyridin-3-yl)-5-fluorophenyl)-N2,N2-dimethylethane-1,2-diamine (1467083-65-3) → 5-(3-((2-(dimethylamino)ethyl)amino)-5-fluorophenyl)pyridine-3,4-diamine (1467083-68-6)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In methanol; at 20 ℃; for 4h;

Reference yield: 88.2%

N1-(3-(4-amino-3-nitropyridin-2-yl)-5-fluorophenyl)-N2,N2-dimethylethane-1,2-diamine → 5-(3-((2-(dimethylamino)ethyl)amino)-5-fluorophenyl)pyridine-3,4-diamine (1467083-68-6)

Guidance literature:

With ammonium chloride; zinc; In methanol; at 20 ℃; for 0.166667h;

Reference yield: 18.4%

N1-(3-(5-amino-4-nitropyridin-3-yl)-5-fluorophenyl)-N2,N2-dimethylethane-1,2-diamine → 5-(3-((2-(dimethylamino)ethyl)amino)-5-fluorophenyl)pyridine-3,4-diamine (1467083-68-6)

Guidance literature:

With palladium on activated charcoal; hydrogen; In methanol; at 20 ℃; for 48h; Inert atmosphere;

upstream raw materials:

4-amino-3-nitropyridine

N¹-(3-(4-amino-5-nitropyridin-3-yl)-5-fluorophenyl)-N²,N²-dimethylethane-1,2-diamine

4-amino-3-bromo-5-nitropyridine

Ν¹-(3-bromo-5-fluorophenyl)-N²,N²-dimethylethane-1,2-diamine

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