pentafluorophenyl 1H-pyrrole-3-butyrate

Base Information

Chemical Name:pentafluorophenyl 1H-pyrrole-3-butyrate
CAS No.:300655-18-9
Molecular Formula:C₁₄H₁₀F₅NO₂
Molecular Weight:319.231
Hs Code.:

Synonyms:pentafluorophenyl 1H-pyrrole-3-butyrate

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Chemical Property of pentafluorophenyl 1H-pyrrole-3-butyrate

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Technology Process of pentafluorophenyl 1H-pyrrole-3-butyrate

There total 3 articles about pentafluorophenyl 1H-pyrrole-3-butyrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 771-61-9
2,3,4,5,6-pentafluorophenol

: 30000-61-4
4-(3-pyrrolyl)butanoic acid

: 300655-18-9
pentafluorophenyl 1H-pyrrole-3-butyrate

Guidance literature:: With dicyclohexyl-carbodiimide; In acetonitrile; at 20 ℃; for 18h;
DOI:10.1039/B001279N

Reference yield:

: 86688-99-5
4-<1-(Phenylsulfonyl)-3-pyrrolyl>butyric acid

: 300655-18-9
pentafluorophenyl 1H-pyrrole-3-butyrate

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / 5 M aq. NaOH / methanol / 5 h / Heating

2: 90 percent / DCC / acetonitrile / 18 h / 20 °C

With sodium hydroxide; dicyclohexyl-carbodiimide; In methanol; acetonitrile;
DOI:10.1039/B001279N

Reference yield:

: 81454-02-6
4-<1-(Phenylsulfonyl)-3-pyrrolyl>-4-oxobutyric acid

: 300655-18-9
pentafluorophenyl 1H-pyrrole-3-butyrate

Guidance literature:: Multi-step reaction with 3 steps

1: 47 percent / amalgamated zinc; conc. HCl / toluene; H₂O / 20 h / Heating

2: 85 percent / 5 M aq. NaOH / methanol / 5 h / Heating

3: 90 percent / DCC / acetonitrile / 18 h / 20 °C

With hydrogenchloride; sodium hydroxide; amalgamated zinc; dicyclohexyl-carbodiimide; In methanol; water; toluene; acetonitrile; 1: Clemmensen reduction;
DOI:10.1039/B001279N