(1β,3β-5Ζ,7Ε)-9,10-secocholesta-5,7,10(19)-triene-1,3,24-triol

Base Information

Chemical Name:(1β,3β-5Ζ,7Ε)-9,10-secocholesta-5,7,10(19)-triene-1,3,24-triol
CAS No.:169218-36-4
Molecular Formula:C₂₇H₄₄O₃
Molecular Weight:416.645
Hs Code.:

Synonyms:(1β,3β-5Ζ,7Ε)-9,10-secocholesta-5,7,10(19)-triene-1,3,24-triol

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Chemical Property of (1β,3β-5Ζ,7Ε)-9,10-secocholesta-5,7,10(19)-triene-1,3,24-triol

Chemical Property:

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Technology Process of (1β,3β-5Ζ,7Ε)-9,10-secocholesta-5,7,10(19)-triene-1,3,24-triol

There total 7 articles about (1β,3β-5Ζ,7Ε)-9,10-secocholesta-5,7,10(19)-triene-1,3,24-triol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₉H₇₂O₃Si₂

: 169218-36-4
(1β,3β-5Ζ,7Ε)-9,10-secocholesta-5,7,10(19)-triene-1,3,24-triol

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 50 - 55 ℃; for 2h;

Reference yield:

: 266686-81-1
C₃₄H₆₀O₅SSi₂

: 169218-36-4
(1β,3β-5Ζ,7Ε)-9,10-secocholesta-5,7,10(19)-triene-1,3,24-triol

Guidance literature:: Multi-step reaction with 5 steps

1: sodium hydrogencarbonate / ethanol / 78 - 85 °C

2: toluene / 110 - 115 °C

3: sodium hydrogencarbonate; sodium persulfate; cetyltrimethylammonium chloride / toluene; water / 60 - 65 °C

4: (1S,2R)-1-amino-2-indanol; potassium tri-sec-butyl-borohydride / tetrahydrofuran / 1 h / -5 - 0 °C / Inert atmosphere

5: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 50 - 55 °C

With sodium persulfate; tetrabutyl ammonium fluoride; cetyltrimethylammonium chloride; sodium hydrogencarbonate; potassium tri-sec-butyl-borohydride; (1S,2R)-1-amino-2-indanol; In tetrahydrofuran; ethanol; water; toluene;

Reference yield:

: C₃₄H₅₈O₂Si

: 169218-36-4
(1β,3β-5Ζ,7Ε)-9,10-secocholesta-5,7,10(19)-triene-1,3,24-triol

Guidance literature:: Multi-step reaction with 8 steps

1.1: 4-nitro-benzoic acid; triphenylphosphine / tetrahydrofuran / Cooling with ice

1.2: 0 °C

2.1: sulfur dioxide / dichloromethane / 1 h / -20 - -10 °C

3.1: ozone / dichloromethane; tetrahydrofuran / -80 - -65 °C

4.1: sodium hydrogencarbonate / ethanol / 78 - 85 °C

5.1: toluene / 110 - 115 °C

6.1: sodium hydrogencarbonate; sodium persulfate; cetyltrimethylammonium chloride / toluene; water / 60 - 65 °C

7.1: (1S,2R)-1-amino-2-indanol; potassium tri-sec-butyl-borohydride / tetrahydrofuran / 1 h / -5 - 0 °C / Inert atmosphere

8.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 50 - 55 °C

With sodium persulfate; sulfur dioxide; tetrabutyl ammonium fluoride; cetyltrimethylammonium chloride; sodium hydrogencarbonate; potassium tri-sec-butyl-borohydride; (1S,2R)-1-amino-2-indanol; ozone; triphenylphosphine; 4-nitro-benzoic acid; In tetrahydrofuran; ethanol; dichloromethane; water; toluene;