(-)-(S)-1-[(benzyloxy)carbonyl]-2-[(R)-5-(methoxycarbonyl)-2-methyl-4-pentenyl]-2,3-dihydropyridine

Base Information

Chemical Name:(-)-(S)-1-[(benzyloxy)carbonyl]-2-[(R)-5-(methoxycarbonyl)-2-methyl-4-pentenyl]-2,3-dihydropyridine
CAS No.:240128-96-5
Molecular Formula:C₂₁H₂₅NO₄
Molecular Weight:355.434
Hs Code.:

Synonyms:(-)-(S)-1-[(benzyloxy)carbonyl]-2-[(R)-5-(methoxycarbonyl)-2-methyl-4-pentenyl]-2,3-dihydropyridine

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Chemical Property of (-)-(S)-1-[(benzyloxy)carbonyl]-2-[(R)-5-(methoxycarbonyl)-2-methyl-4-pentenyl]-2,3-dihydropyridine

Chemical Property:

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Technology Process of (-)-(S)-1-[(benzyloxy)carbonyl]-2-[(R)-5-(methoxycarbonyl)-2-methyl-4-pentenyl]-2,3-dihydropyridine

There total 9 articles about (-)-(S)-1-[(benzyloxy)carbonyl]-2-[(R)-5-(methoxycarbonyl)-2-methyl-4-pentenyl]-2,3-dihydropyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₁H₂₇NO₅

: 240128-96-5
(-)-(S)-1-[(benzyloxy)carbonyl]-2-[(R)-5-(methoxycarbonyl)-2-methyl-4-pentenyl]-2,3-dihydropyridine

Guidance literature:: With dmap; methanesulfonyl chloride; In dichloromethane; water;
DOI:10.1021/ol990028j

Reference yield:

: 240128-95-4
(-)-(S)-1-[(benzyloxy)carbonyl]-2-[(R)-2-methyl-4-pentenyl]-2,3-dihydro-4-pyridone

: 240128-96-5
(-)-(S)-1-[(benzyloxy)carbonyl]-2-[(R)-5-(methoxycarbonyl)-2-methyl-4-pentenyl]-2,3-dihydropyridine

Guidance literature:: Multi-step reaction with 4 steps

1: 84 percent / NaIO₄; OsO₄

2: 89 percent / t-BuOK / tetrahydrofuran

3: NaBH₄; CeCl₃

4: MsCl; DMAP / CH₂Cl₂; H₂O

With dmap; sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; cerium(III) chloride; potassium tert-butylate; methanesulfonyl chloride; In tetrahydrofuran; dichloromethane; water; 2: Horner-Wadsworth-Emmons olefination / 3: Luche reduction;
DOI:10.1021/ol990028j

Reference yield:

: 240129-06-0
(-)-(S)-1-[(benzyloxy)carbonyl]-2-[(S)-2-methyl-4-oxobutyl]-2,3-dihydro-4-pyridone

: 240128-96-5
(-)-(S)-1-[(benzyloxy)carbonyl]-2-[(R)-5-(methoxycarbonyl)-2-methyl-4-pentenyl]-2,3-dihydropyridine

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / t-BuOK / tetrahydrofuran

2: NaBH₄; CeCl₃

3: MsCl; DMAP / CH₂Cl₂; H₂O

With dmap; sodium tetrahydroborate; cerium(III) chloride; potassium tert-butylate; methanesulfonyl chloride; In tetrahydrofuran; dichloromethane; water; 1: Horner-Wadsworth-Emmons olefination / 2: Luche reduction;
DOI:10.1021/ol990028j