Technology Process of C45H40N6O12
There total 4 articles about C45H40N6O12 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tetrakis(actonitrile)copper(I) hexafluorophosphate;
In
dichloromethane; water; tert-butyl alcohol;
at 60 ℃;
for 4h;
Microwave irradiation;
DOI:10.1016/j.carres.2012.10.001
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium hydride / N,N-dimethyl-formamide
2: toluene-4-sulfonic acid / methanol
3: sodium hydride / N,N-dimethyl-formamide
4: tetrakis(actonitrile)copper(I) hexafluorophosphate / water; tert-butyl alcohol; dichloromethane / 4 h / 60 °C / Microwave irradiation
With
tetrakis(actonitrile)copper(I) hexafluorophosphate; sodium hydride; toluene-4-sulfonic acid;
In
methanol; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol;
1: |Williamson Ether Synthesis / 4: |Huisgen Cycloaddition;
DOI:10.1016/j.carres.2012.10.001
- Guidance literature:
-
Multi-step reaction with 3 steps
1: toluene-4-sulfonic acid / methanol
2: sodium hydride / N,N-dimethyl-formamide
3: tetrakis(actonitrile)copper(I) hexafluorophosphate / water; tert-butyl alcohol; dichloromethane / 4 h / 60 °C / Microwave irradiation
With
tetrakis(actonitrile)copper(I) hexafluorophosphate; sodium hydride; toluene-4-sulfonic acid;
In
methanol; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol;
3: |Huisgen Cycloaddition;
DOI:10.1016/j.carres.2012.10.001