N-[2-(3,4-dimethoxyphenyl)ethyl]-2-ethylsulfenyl-N-(2-methylpropenyl)acetamide

Base Information

• Chemical Name: N-[2-(3,4-dimethoxyphenyl)ethyl]-2-ethylsulfenyl-N-(2-methylpropenyl)acetamide
• CAS No.: 459831-96-0
• Molecular Formula: C₁₈H₂₇NO₃S
• Molecular Weight: 337.483

Synonyms:N-[2-(3,4-dimethoxyphenyl)ethyl]-2-ethylsulfenyl-N-(2-methylpropenyl)acetamide

Chemical Property of N-[2-(3,4-dimethoxyphenyl)ethyl]-2-ethylsulfenyl-N-(2-methylpropenyl)acetamide

Chemical Property:

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Technology Process of N-[2-(3,4-dimethoxyphenyl)ethyl]-2-ethylsulfenyl-N-(2-methylpropenyl)acetamide

There total 2 articles about N-[2-(3,4-dimethoxyphenyl)ethyl]-2-ethylsulfenyl-N-(2-methylpropenyl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

2-(ethylthio)acetyl chloride (54256-37-0) + [2-(3,4-dimethoxyphenyl)ethyl](isobutylidene)amine (459831-95-9) → N-[2-(3,4-dimethoxyphenyl)ethyl]-2-ethylsulfenyl-N-(2-methylpropenyl)acetamide (459831-96-0)

Guidance literature:

With pyridine; In dichloromethane; at 25 ℃; for 12h;

DOI:10.1021/jo020083x

Reference yield:

2-(3,4-dimethoxyphenyl)-ethylamine (120-20-7) → N-[2-(3,4-dimethoxyphenyl)ethyl]-2-ethylsulfenyl-N-(2-methylpropenyl)acetamide (459831-96-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 80 percent / 1.5 h / 0 - 25 °C

2: 62 percent / pyridine / CH₂Cl₂ / 12 h / 25 °C

With pyridine; In dichloromethane;

DOI:10.1021/jo020083x

Reference yield: 72.0%

N-[2-(3,4-dimethoxyphenyl)ethyl]-2-ethylsulfenyl-N-(2-methylpropenyl)acetamide (459831-96-0) → N-[2-(3,4-dimethoxyphenyl)ethyl]-2-ethylsulfinyl-N-(2-methylpropenyl)acetamide (459831-75-5)

Guidance literature:

With sodium periodate; In methanol; water; at 20 ℃; for 3h;

DOI:10.1021/jo020083x

upstream raw materials:

2-(ethylthio)acetyl chloride

[2-(3,4-dimethoxyphenyl)ethyl](isobutylidene)amine

2-(3,4-dimethoxyphenyl)-ethylamine

Downstream raw materials:

N-[2-(3,4-dimethoxyphenyl)ethyl]-2-ethylsulfinyl-N-(2-methylpropenyl)acetamide

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