(4R,5R)-methyl 4-O-benzoyl-5-[1'-(dimethoxyphosphinyl)-2'-methoxy-2'-oxo-ethoxy]cyclohex-1-ene-carboxylate

Base Information

Chemical Name:(4R,5R)-methyl 4-O-benzoyl-5-[1'-(dimethoxyphosphinyl)-2'-methoxy-2'-oxo-ethoxy]cyclohex-1-ene-carboxylate
CAS No.:1173095-36-7
Molecular Formula:C₂₀H₂₅O₁₀P
Molecular Weight:456.386
Hs Code.:

Synonyms:(4R,5R)-methyl 4-O-benzoyl-5-[1'-(dimethoxyphosphinyl)-2'-methoxy-2'-oxo-ethoxy]cyclohex-1-ene-carboxylate

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Chemical Property of (4R,5R)-methyl 4-O-benzoyl-5-[1'-(dimethoxyphosphinyl)-2'-methoxy-2'-oxo-ethoxy]cyclohex-1-ene-carboxylate

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Technology Process of (4R,5R)-methyl 4-O-benzoyl-5-[1'-(dimethoxyphosphinyl)-2'-methoxy-2'-oxo-ethoxy]cyclohex-1-ene-carboxylate

There total 1 articles about (4R,5R)-methyl 4-O-benzoyl-5-[1'-(dimethoxyphosphinyl)-2'-methoxy-2'-oxo-ethoxy]cyclohex-1-ene-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 1173095-35-6
(4R,5R)-methyl-4-benzoyloxy-5-hydroxy-1-cyclohexene-1-carboxylate

: 60190-78-5
methyl 2-diazo-2-(dimethoxyphosphoryl)acetate

: 1173095-36-7
(4R,5R)-methyl 4-O-benzoyl-5-[1'-(dimethoxyphosphinyl)-2'-methoxy-2'-oxo-ethoxy]cyclohex-1-ene-carboxylate

Guidance literature:: With dirhodium tetraacetate; In benzene; at 85 ℃; for 24h; Inert atmosphere;
DOI:10.1039/b901694e

Reference yield: 100.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 1173095-36-7
(4R,5R)-methyl 4-O-benzoyl-5-[1'-(dimethoxyphosphinyl)-2'-methoxy-2'-oxo-ethoxy]cyclohex-1-ene-carboxylate

: 1173095-37-8
C₁₉H₂₀O₇

Guidance literature:: (4R,5R)-methyl 4-O-benzoyl-5-[1'-(dimethoxyphosphinyl)-2'-methoxy-2'-oxo-ethoxy]cyclohex-1-ene-carboxylate; With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 0.166667h; Inert atmosphere;

formaldehyd; In tetrahydrofuran; at -78 ℃;
DOI:10.1039/b901694e