(E)-2-(2-(benzo[d]thiazol-2-yl)-2-(cyano)vinyl)-5-(diethylamino)phenyl diethyl phosphate

Base Information

Chemical Name:(E)-2-(2-(benzo[d]thiazol-2-yl)-2-(cyano)vinyl)-5-(diethylamino)phenyl diethyl phosphate
CAS No.:1335289-87-6
Molecular Formula:C₂₄H₂₈N₃O₄PS
Molecular Weight:485.544
Hs Code.:

Synonyms:(E)-2-(2-(benzo[d]thiazol-2-yl)-2-(cyano)vinyl)-5-(diethylamino)phenyl diethyl phosphate

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Chemical Property of (E)-2-(2-(benzo[d]thiazol-2-yl)-2-(cyano)vinyl)-5-(diethylamino)phenyl diethyl phosphate

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Technology Process of (E)-2-(2-(benzo[d]thiazol-2-yl)-2-(cyano)vinyl)-5-(diethylamino)phenyl diethyl phosphate

There total 2 articles about (E)-2-(2-(benzo[d]thiazol-2-yl)-2-(cyano)vinyl)-5-(diethylamino)phenyl diethyl phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 56278-50-3
2-cyanomethylbenzothiazole

: 1335289-86-5
C₁₅H₂₄NO₅P

: 1335289-87-6
(E)-2-(2-(benzo[d]thiazol-2-yl)-2-(cyano)vinyl)-5-(diethylamino)phenyl diethyl phosphate

Guidance literature:: With piperidine; In ethanol; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1039/c1cc13819g

Reference yield:

: 17754-90-4
4-(Diethylamino)salicylaldehyde

: 1335289-87-6
(E)-2-(2-(benzo[d]thiazol-2-yl)-2-(cyano)vinyl)-5-(diethylamino)phenyl diethyl phosphate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / tetrahydrofuran; mineral oil / 24 h / 20 °C / Inert atmosphere

2: piperidine / ethanol / 1 h / 20 °C / Inert atmosphere

With piperidine; sodium hydride; In tetrahydrofuran; ethanol; mineral oil;
DOI:10.1039/c1cc13819g

Reference yield: 44.0%

: 1335289-87-6
(E)-2-(2-(benzo[d]thiazol-2-yl)-2-(cyano)vinyl)-5-(diethylamino)phenyl diethyl phosphate

: sodium (E)-2-(2-(benzo[d]thiazol-2-yl)-2-(cyano)vinyl)-5-(diethylamino)phenyl phosphate

Guidance literature:: (E)-2-(2-(benzo[d]thiazol-2-yl)-2-(cyano)vinyl)-5-(diethylamino)phenyl diethyl phosphate; With trimethylsilyl bromide; In dichloromethane; at 20 ℃; for 8h; Inert atmosphere;

With sodium hydroxide; In water; pH=9 - 10;
DOI:10.1039/c1cc13819g