(2S,3S)-6-(t-butyldimethylsilyloxy)-2-((4S,5S,E)-4-(1-ethoxyethoxy)-6-(4-methoxybenzyloxy)-5-methylhex-1-enyl)-3,6-dihydro-2H-pyran-3-yl pivalate

Base Information

Chemical Name:(2S,3S)-6-(t-butyldimethylsilyloxy)-2-((4S,5S,E)-4-(1-ethoxyethoxy)-6-(4-methoxybenzyloxy)-5-methylhex-1-enyl)-3,6-dihydro-2H-pyran-3-yl pivalate
CAS No.:1208114-29-7
Molecular Formula:C₃₅H₅₈O₈Si
Molecular Weight:634.926
Hs Code.:

Synonyms:(2S,3S)-6-(t-butyldimethylsilyloxy)-2-((4S,5S,E)-4-(1-ethoxyethoxy)-6-(4-methoxybenzyloxy)-5-methylhex-1-enyl)-3,6-dihydro-2H-pyran-3-yl pivalate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3S)-6-(t-butyldimethylsilyloxy)-2-((4S,5S,E)-4-(1-ethoxyethoxy)-6-(4-methoxybenzyloxy)-5-methylhex-1-enyl)-3,6-dihydro-2H-pyran-3-yl pivalate

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Technology Process of (2S,3S)-6-(t-butyldimethylsilyloxy)-2-((4S,5S,E)-4-(1-ethoxyethoxy)-6-(4-methoxybenzyloxy)-5-methylhex-1-enyl)-3,6-dihydro-2H-pyran-3-yl pivalate

There total 1 articles about (2S,3S)-6-(t-butyldimethylsilyloxy)-2-((4S,5S,E)-4-(1-ethoxyethoxy)-6-(4-methoxybenzyloxy)-5-methylhex-1-enyl)-3,6-dihydro-2H-pyran-3-yl pivalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1208114-26-4
(2S,3R)-6-(t-butyldimethylsilyloxy)-2-((4S,5S,E)-4-(1-ethoxyethoxy)-6-(4-methoxybenzyloxy)-5-methylhex-1-enyl)-3,6-dihydro-2H-pyran-3-ol

: 75-98-9
Trimethylacetic acid

: 1208114-29-7
(2S,3S)-6-(t-butyldimethylsilyloxy)-2-((4S,5S,E)-4-(1-ethoxyethoxy)-6-(4-methoxybenzyloxy)-5-methylhex-1-enyl)-3,6-dihydro-2H-pyran-3-yl pivalate

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 0 - 20 ℃;
DOI:10.1021/ja9097252

Reference yield:

: 1208114-29-7
(2S,3S)-6-(t-butyldimethylsilyloxy)-2-((4S,5S,E)-4-(1-ethoxyethoxy)-6-(4-methoxybenzyloxy)-5-methylhex-1-enyl)-3,6-dihydro-2H-pyran-3-yl pivalate

: 1240018-03-4
C₃₀H₅₀O₇Si

Guidance literature:: (2S,3S)-6-(t-butyldimethylsilyloxy)-2-((4S,5S,E)-4-(1-ethoxyethoxy)-6-(4-methoxybenzyloxy)-5-methylhex-1-enyl)-3,6-dihydro-2H-pyran-3-yl pivalate; With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; for 2h; Inert atmosphere;

With water; In tetrahydrofuran; at 0 ℃; Inert atmosphere;
DOI:10.1021/jo1010203