Technology Process of C14H20N2O2
There total 6 articles about C14H20N2O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C18H30N2O3;
With
thionyl chloride;
In
tetrahydrofuran;
at 20 ℃;
With
sodium hydrogencarbonate;
In
water;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: aluminum (III) chloride / dichloromethane / -30 - 20 °C
2: hydroxylamine hydrochloride; sodium acetate / ethanol / 4 h / Reflux
3: hydrogen / palladium 10% on activated carbon / ethanol / 4137.29 Torr
4: triethylamine / dichloromethane / 2 h
5: sodium tetrahydroborate / ethanol / 3 h / 20 - 50 °C
6: thionyl chloride / tetrahydrofuran / 20 °C
With
aluminum (III) chloride; sodium tetrahydroborate; thionyl chloride; hydroxylamine hydrochloride; hydrogen; sodium acetate; triethylamine;
palladium 10% on activated carbon;
In
tetrahydrofuran; ethanol; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: hydroxylamine hydrochloride; sodium acetate / ethanol / 4 h / Reflux
2: hydrogen / palladium 10% on activated carbon / ethanol / 4137.29 Torr
3: triethylamine / dichloromethane / 2 h
4: sodium tetrahydroborate / ethanol / 3 h / 20 - 50 °C
5: thionyl chloride / tetrahydrofuran / 20 °C
With
sodium tetrahydroborate; thionyl chloride; hydroxylamine hydrochloride; hydrogen; sodium acetate; triethylamine;
palladium 10% on activated carbon;
In
tetrahydrofuran; ethanol; dichloromethane;
