4-amino-4'-ferrocenyl-2,3'-dimethylazobenzene

Base Information

• Chemical Name: 4-amino-4'-ferrocenyl-2,3'-dimethylazobenzene
• CAS No.: 220082-14-4
• Molecular Formula: C₂₄H₂₃FeN₃
• Molecular Weight: 409.314

Synonyms:4-amino-4'-ferrocenyl-2,3'-dimethylazobenzene

Chemical Property of 4-amino-4'-ferrocenyl-2,3'-dimethylazobenzene

Chemical Property:

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Technology Process of 4-amino-4'-ferrocenyl-2,3'-dimethylazobenzene

There total 1 articles about 4-amino-4'-ferrocenyl-2,3'-dimethylazobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

sodium sulfide hydrate + 4-nitro-2-methyl-3'-methyl-4'-ferrocenylazobenzene → 4-amino-4'-ferrocenyl-2,3'-dimethylazobenzene (220082-14-4)

Guidance literature:

In ethanol; N2-atmosphere; refluxing (1 h); solvent removal (vac.), chromy. (SiO2, CH2Cl2), concn., crystn. on pentane addn.; elem. anal.;

DOI:10.1039/DT9940003427

Reference yield: 70.0%

4-amino-4'-ferrocenyl-2,3'-dimethylazobenzene (220082-14-4) + MoCl2(HB(N2C3H2C6H4OCH3)3)(NO) → Mo(Cl)(HB(N2C3H2C6H4OCH3)3)(NO)NHC6H3(CH3)N2C6H3(CH3)(C5H4)Fe(C5H5)

Guidance literature:

With triethylamine; In toluene; N2; mixt. refluxing for 5 h, cooling, evapn. to dryness under reduced pressure; column chromy. (silica gel, 1% THF/CH2Cl2); elem. anal.;

DOI:10.1021/jp982764v

Reference yield: 35.0%

4-amino-4'-ferrocenyl-2,3'-dimethylazobenzene (220082-14-4) + 2-nitroso-5-nitrotoluene (57610-10-3) → 4'-ferrocenyl-2,3'-dimethyl-4-(2-methyl-4-nitrophenylazo)azobenzene* 0.1 CH2Cl2

Guidance literature:

In acetic acid; N2-atmosphere; molar ratio Fe-complex:ligand=73:151, stirring (in CH3COOH:H2O=1:2 (v/v), room temp., 24 h); addn. of water and CH2Cl2, shaking, sepn. of org. layer, extn. of water layer into CH2Cl2, evapn. of combined org. layers to dryness, chromy. (SiO2, CH2Cl2), evapn.; elem. anal.;

DOI:10.1039/DT9940003427

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