1',3'-Dihydro-1',1',3',3'-tetraphenyldispiro<1,3>diphosphole-5',1-cyclopropane>-1',3'-diium diiodide

Base Information

Chemical Name:1',3'-Dihydro-1',1',3',3'-tetraphenyldispiro<1,3>diphosphole-5',1-cyclopropane>-1',3'-diium diiodide
CAS No.:123542-08-5
Molecular Formula:C₃₁H₃₀P₂*2I
Molecular Weight:718.336
Hs Code.:

1',3'-Dihydro-1',1',3',3'-tetraphenyldispiro<cyclopropane-1,4'<2H><1,3>diphosphole-5',1-cyclopropane>-1',3'-diium diiodide

Synonyms:1',3'-Dihydro-1',1',3',3'-tetraphenyldispiro<1,3>diphosphole-5',1-cyclopropane>-1',3'-diium diiodide

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Chemical Property of 1',3'-Dihydro-1',1',3',3'-tetraphenyldispiro<1,3>diphosphole-5',1-cyclopropane>-1',3'-diium diiodide

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Technology Process of 1',3'-Dihydro-1',1',3',3'-tetraphenyldispiro<1,3>diphosphole-5',1-cyclopropane>-1',3'-diium diiodide

There total 3 articles about 1',3'-Dihydro-1',1',3',3'-tetraphenyldispiro<1,3>diphosphole-5',1-cyclopropane>-1',3'-diium diiodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 75-11-6
diiodomethane

: 123542-06-3
1,1'-Bis(diphenylphosphino)bicyclopropyl

: 123542-08-5
1',3'-Dihydro-1',1',3',3'-tetraphenyldispiro<1,3>diphosphole-5',1-cyclopropane>-1',3'-diium diiodide

Guidance literature:: In chloroform; for 720h; Ambient temperature;

Reference yield:

: 113017-77-9
2,3-dibuta-1,3-diene

: 123542-08-5
1',3'-Dihydro-1',1',3',3'-tetraphenyldispiro<1,3>diphosphole-5',1-cyclopropane>-1',3'-diium diiodide

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) sodium hydride / 1.) DMSO, 1 h, room temperature, 2.) 2 h, 70 deg C

2: 43 percent / HSiCl₃, NEt₃ / toluene / 3 h / Heating

3: 73 percent / CHCl₃ / 720 h / Ambient temperature

With trichlorosilane; sodium hydride; triethylamine; In chloroform; toluene;

Reference yield:

: 123542-05-2
1,1'-Bis(diphenylphosphinyl)bicyclopropyl

: 123542-08-5
1',3'-Dihydro-1',1',3',3'-tetraphenyldispiro<1,3>diphosphole-5',1-cyclopropane>-1',3'-diium diiodide

Guidance literature:: Multi-step reaction with 2 steps

1: 43 percent / HSiCl₃, NEt₃ / toluene / 3 h / Heating

2: 73 percent / CHCl₃ / 720 h / Ambient temperature

With trichlorosilane; triethylamine; In chloroform; toluene;