<2-D1>Biphenyl

Base Information

• Chemical Name: <2-D1>Biphenyl
• CAS No.: 4819-96-9
• Molecular Formula: C₁₂H₁₀
• Molecular Weight: 155.203

Synonyms:<2-D1>Biphenyl

Chemical Property of <2-D1>Biphenyl

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of <2-D1>Biphenyl

There total 2 articles about <2-D1>Biphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 14.3%

dibenzothiophene (132-65-0) → biphenyl (92-52-4,1594-86-1) + 2,2'-bisdeuterium-1,1'-biphenyl (16327-75-6) + <2-D1>Biphenyl (4819-96-9)

Guidance literature:

With [2,2]bipyridinyl; bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; lithium aluminium deuteride; In tetrahydrofuran; at 55 ℃; for 48h;

DOI:10.1021/ja00284a045

Reference yield:

(1,3-bis(2,6-diisopropylphenyl)-imidazol-2-ylidene)Au(biphenyl)Cl → bisbenzocyclobutene (259-79-0) + <2-D1>Biphenyl (4819-96-9)

Guidance literature:

(1,3-bis(2,6-diisopropylphenyl)-imidazol-2-ylidene)Au(biphenyl)Cl; With lithium triethyl borodeuteride; In tetrahydrofuran; toluene; at -90 - 20 ℃; Schlenk technique;

With water; ammonium chloride;

DOI:10.1039/d1dt01315g

Reference yield:

potassium graphite + UI(NCtBuMes)3(DME) + <2-D1>Biphenyl (4819-96-9) → K2[(μ-η6,η6-biphenyl-2-d1)[U(NCtBuMes)3]2]

Guidance literature:

In 1,2-dimethoxyethane; (drybox, Schlenk, Ar) KC8 in DME was frozen, the thawing slurry was added dropwise to a frozen soln. of U-complex and biphenyl in DME, the mixt.was stirred at ca. 25°C for 25 min; filtered, the solvent was removed, extd. with pentane, filtered, evapd. to dryness, mixed with diethyl ether, stored for several days at -35°C, decanted, dried;

DOI:10.1021/ic202163m

upstream raw materials:

dibenzothiophene

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 4819-96-9 <2-D1>Biphenyl

Send

Send

Metric Ton KG G Pound L ML

Send

Send