2,3-Dihydroimidazo(1,2-f)phenanthridine

Base Information

• Chemical Name: 2,3-Dihydroimidazo(1,2-f)phenanthridine
• CAS No.: 36811-70-8
• Molecular Formula: C₁₅H₁₂N₂
• Molecular Weight: 220.274
• NSC Number: 141590
• UNII: W6SAN3C3Y7
• DSSTox Substance ID: DTXSID70958024
• Wikidata: Q82938527
• ChEMBL ID: CHEMBL1181670
• Mol file: 36811-70-8.mol

Synonyms:2,3-Dihydroimidazo(1,2-f)phenanthridine;2,3-Dihydroimidazo[1,2-f]phenanthridine;36811-70-8;W6SAN3C3Y7;MLS002920530;NSC141590;UNII-W6SAN3C3Y7;NSC 141590;NSC-141590;SMR001798119;Imidazo[1,2-f]phenanthridine, 2,3-dihydro-;IMIDAZO(1,2-F)PHENANTHRIDINE, 2,3-DIHYDRO-;Imidazo[1, 2,3-dihydro-;cid_285026;CHEMBL1181670;BDBM83852;DTXSID70958024;NCI60_000914;{Imidazo[1,2-f]phenanthridine,} 2,3-dihydro-;SR-01000885430;SR-01000885430-2

Chemical Property of 2,3-Dihydroimidazo(1,2-f)phenanthridine

Chemical Property:

• Vapor Pressure: 3.68E-07mmHg at 25°C
• Boiling Point: 416.9°C at 760 mmHg
• Flash Point: 206°C
• Density: 1.25g/cm³
• XLogP3: 2.3
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 0
• Exact Mass: 220.100048391
• Heavy Atom Count: 17
• Complexity: 336

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1CN2C3=CC=CC=C3C4=CC=CC=C4C2=N1

Technology Process of 2,3-Dihydroimidazo(1,2-f)phenanthridine

There total 4 articles about 2,3-Dihydroimidazo(1,2-f)phenanthridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C15H14N2 (885107-95-9) → 2,3-dihydro-imidazo[1,2-f]phenanthridine (36811-70-8)

Guidance literature:

With manganese(IV) oxide; sodium carbonate; at -78 - 20 ℃; for 2h;

DOI:10.1039/b517117b

Reference yield:

5-(2-bromo-ethyl)-phenanthridinium bromide → 2,3-dihydro-imidazo[1,2-f]phenanthridine (36811-70-8)

Guidance literature:

Multi-step reaction with 2 steps

1: NH₃ / 1 h / -30 °C

2: Na₂CO₃; MnO₂ / 2 h / -78 - 20 °C

With manganese(IV) oxide; ammonia; sodium carbonate;

DOI:10.1039/b517117b

Reference yield:

phenanthridine (229-87-8) → 2,3-dihydro-imidazo[1,2-f]phenanthridine (36811-70-8)

Guidance literature:

Multi-step reaction with 3 steps

1: 95 percent / 120 h / 90 °C

2: NH₃ / 1 h / -30 °C

3: Na₂CO₃; MnO₂ / 2 h / -78 - 20 °C

With manganese(IV) oxide; ammonia; sodium carbonate;

DOI:10.1039/b517117b

upstream raw materials:

C₁₅H₁₄N₂

phenanthridine

Downstream raw materials:

imidazo[1,2-f]phenanthridine