N-(2,5-dimethoxy-phenyl)-4,6-bis-octyloxy-isophthalamic acid methyl ester

Base Information

Chemical Name:N-(2,5-dimethoxy-phenyl)-4,6-bis-octyloxy-isophthalamic acid methyl ester
CAS No.:866482-44-2
Molecular Formula:C₃₃H₄₉NO₇
Molecular Weight:571.755
Hs Code.:

<i>N</i>-(2,5-dimethoxy-phenyl)-4,6-bis-octyloxy-isophthalamic acid methyl ester

Synonyms:N-(2,5-dimethoxy-phenyl)-4,6-bis-octyloxy-isophthalamic acid methyl ester

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Chemical Property of N-(2,5-dimethoxy-phenyl)-4,6-bis-octyloxy-isophthalamic acid methyl ester

Chemical Property:

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Technology Process of N-(2,5-dimethoxy-phenyl)-4,6-bis-octyloxy-isophthalamic acid methyl ester

There total 4 articles about N-(2,5-dimethoxy-phenyl)-4,6-bis-octyloxy-isophthalamic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 89-39-4
1,4-dimethoxy-2-nitrobenzene

: 866482-44-2
N-(2,5-dimethoxy-phenyl)-4,6-bis-octyloxy-isophthalamic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / hydrogen / Pd/C / tetrahydrofuran / 8 h / 20 °C / 760 Torr

2: 1.84 g / triethylamine / CHCl₃ / 10 h / 20 °C

With hydrogen; triethylamine; palladium on activated charcoal; In tetrahydrofuran; chloroform;
DOI:10.1039/b508773b

Reference yield:

: 866482-43-1
5-chlorocarbonyl-2,4-bis-octyloxy-benzoic acid methyl ester

: 102-56-7,102526-87-4
2,5-dimethoxyaniline

: 866482-44-2
N-(2,5-dimethoxy-phenyl)-4,6-bis-octyloxy-isophthalamic acid methyl ester

Guidance literature:: With triethylamine; In chloroform; at 20 ℃; for 10h;
DOI:10.1039/b508773b

Reference yield:

: 345625-94-7
4,6-bis-octyloxyisophthalic acid monomethyl ester

: 866482-44-2
N-(2,5-dimethoxy-phenyl)-4,6-bis-octyloxy-isophthalamic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl chloride; DMF / CH₂Cl₂ / 5 h / 20 °C

2: 1.84 g / triethylamine / CHCl₃ / 10 h / 20 °C

With oxalyl dichloride; triethylamine; N,N-dimethyl-formamide; In dichloromethane; chloroform;
DOI:10.1039/b508773b