N-2-(2-tetrahydropyranyloxy)ethyl-3-(3,5-di-tert-butyl-4-hydroxybenzylidene)-2-pyrrolidone

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Chemical Name:N-2-(2-tetrahydropyranyloxy)ethyl-3-(3,5-di-tert-butyl-4-hydroxybenzylidene)-2-pyrrolidone
CAS No.:110027-14-0
Molecular Formula:C₂₆H₃₉NO₄
Molecular Weight:429.6
Hs Code.:

Synonyms:N-2-(2-tetrahydropyranyloxy)ethyl-3-(3,5-di-tert-butyl-4-hydroxybenzylidene)-2-pyrrolidone

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Chemical Property of N-2-(2-tetrahydropyranyloxy)ethyl-3-(3,5-di-tert-butyl-4-hydroxybenzylidene)-2-pyrrolidone

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Technology Process of N-2-(2-tetrahydropyranyloxy)ethyl-3-(3,5-di-tert-butyl-4-hydroxybenzylidene)-2-pyrrolidone

There total 3 articles about N-2-(2-tetrahydropyranyloxy)ethyl-3-(3,5-di-tert-butyl-4-hydroxybenzylidene)-2-pyrrolidone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 106221-56-1
N-acetyl-3-(3,5-di-tert-butyl-4-hydroxybenzylidene)pyrrolidin-2-one

: 110027-14-0
N-<2-<(2-tetrahydropyranyl)oxy>ethyl>-3-(3,5-di-tert-butyl-4-hydroxybenzylidene)pyrrolidin-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: 12.7 g / K₂CO₃ / ethanol; methanol / 1 h / Ambient temperature

2: 190 mg / NaH / dimethylformamide / 1 h / Ambient temperature

With sodium hydride; potassium carbonate; In methanol; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00394a011

Reference yield:

: 1620-98-0
3,5-di-t-butyl-4-hydroxybenzaldehyde

: 110027-14-0
N-<2-<(2-tetrahydropyranyl)oxy>ethyl>-3-(3,5-di-tert-butyl-4-hydroxybenzylidene)pyrrolidin-2-one

Guidance literature:: Multi-step reaction with 3 steps

1: 22 g / Et₃N / ethanol / 2 h / 60 °C

2: 12.7 g / K₂CO₃ / ethanol; methanol / 1 h / Ambient temperature

3: 190 mg / NaH / dimethylformamide / 1 h / Ambient temperature

With sodium hydride; potassium carbonate; triethylamine; In methanol; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00394a011