acide phenyl-2 (methyl-4 phenyl)-2 hydroxy-2 ethanoique

Base Information

Chemical Name:acide phenyl-2 (methyl-4 phenyl)-2 hydroxy-2 ethanoique
CAS No.:51999-09-8
Molecular Formula:C₁₅H₁₄O₃
Molecular Weight:242.274
Hs Code.:

Synonyms:acide phenyl-2 (methyl-4 phenyl)-2 hydroxy-2 ethanoique

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Chemical Property of acide phenyl-2 (methyl-4 phenyl)-2 hydroxy-2 ethanoique

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Technology Process of acide phenyl-2 (methyl-4 phenyl)-2 hydroxy-2 ethanoique

There total 12 articles about acide phenyl-2 (methyl-4 phenyl)-2 hydroxy-2 ethanoique which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1042740-62-4
(R)-benzyl 2-hydroxy-2-(4-methylphenyl)-phenylacetate

: 51999-09-8
acide phenyl-2 (methyl-4 phenyl)-2 hydroxy-2 ethanoique

Guidance literature:: With sodium hydroxide; water; In methanol; for 4h; Reflux;
DOI:10.1002/anie.200800423

Reference yield:

: 63007-15-8
trans-(4S,5S)-2-benzoyl-4-(methoxymethyl)-5-phenyl-2-oxazoline

: 51999-09-8
acide phenyl-2 (methyl-4 phenyl)-2 hydroxy-2 ethanoique

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / tetrahydrofuran / -78 °C

2: 1) MeI 2) KOH / 1) DMSO, r.t 2) reflux, 8h (other reagent, other solvent)

With potassium hydroxide; methyl iodide; In tetrahydrofuran;
DOI:10.1021/jo01302a008

Reference yield:

: 58635-82-8
(S,S)-2-benzyl-4-methoxymethyl-5-phenyl-2-oxazoline

: 51999-09-8
acide phenyl-2 (methyl-4 phenyl)-2 hydroxy-2 ethanoique

Guidance literature:: Multi-step reaction with 3 steps

1: 1) Lithium diisopropylamide 2)O₂ / 1) THF, -78 deg C, 2h 2) ether, -78 deg C, 1h

2: 93 percent / tetrahydrofuran / -78 °C

3: 1) MeI 2) KOH / 1) DMSO, r.t 2) reflux, 8h (other reagent, other solvent)

With potassium hydroxide; oxygen; lithium diisopropyl amide; methyl iodide; In tetrahydrofuran;
DOI:10.1021/jo01302a008