3-benzyloxy-6-methylpyran-4(1H)-one-2-carboxy-N-(4,4-cyanophenylbenzylamide)

Base Information

Chemical Name:3-benzyloxy-6-methylpyran-4(1H)-one-2-carboxy-N-(4,4-cyanophenylbenzylamide)
CAS No.:932025-43-9
Molecular Formula:C₂₈H₂₂N₂O₄
Molecular Weight:450.494
Hs Code.:

Synonyms:3-benzyloxy-6-methylpyran-4(1H)-one-2-carboxy-N-(4,4-cyanophenylbenzylamide)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-benzyloxy-6-methylpyran-4(1H)-one-2-carboxy-N-(4,4-cyanophenylbenzylamide)

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Technology Process of 3-benzyloxy-6-methylpyran-4(1H)-one-2-carboxy-N-(4,4-cyanophenylbenzylamide)

There total 3 articles about 3-benzyloxy-6-methylpyran-4(1H)-one-2-carboxy-N-(4,4-cyanophenylbenzylamide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 868368-24-5
3-benzyloxy-6-methylpyran-4(1H)-one-2-carboxy-N-(4-iodobenzylamide)

: 126747-14-6
4-cyanophenylboronic acid

: 932025-43-9
3-benzyloxy-6-methylpyran-4(1H)-one-2-carboxy-N-(4,4-cyanophenylbenzylamide)

Guidance literature:: With palladium diacetate; potassium carbonate; triphenylphosphine; In toluene; at 135 ℃; for 240h;
DOI:10.1021/ja054558o

Reference yield:

: 3-benzyloxy-6-methyl-4-oxo-4H-pyran-2-carboxylic acid 2,5-dioxo-pyrrolidin-1-yl ester

: 932025-43-9
3-benzyloxy-6-methylpyran-4(1H)-one-2-carboxy-N-(4,4-cyanophenylbenzylamide)

Guidance literature:: Multi-step reaction with 2 steps

1: 3 g / tetrahydrofuran / 60 °C

2: 40 percent / aq. K₂CO₃; Pd(OAc)2; PPh₃ / toluene / 240 h / 135 °C

With palladium diacetate; potassium carbonate; triphenylphosphine; In tetrahydrofuran; toluene;
DOI:10.1021/ja054558o

Reference yield:

: 216581-47-4
3-(benzyloxy)-6-methyl-4-oxo-4H-pyran-2-carboxylic acid

: 932025-43-9
3-benzyloxy-6-methylpyran-4(1H)-one-2-carboxy-N-(4,4-cyanophenylbenzylamide)

Guidance literature:: Multi-step reaction with 3 steps

1: 1,3-dicyclohexylcarbodiimide / tetrahydrofuran / 3 h / 20 °C

2: 3 g / tetrahydrofuran / 60 °C

3: 40 percent / aq. K₂CO₃; Pd(OAc)2; PPh₃ / toluene / 240 h / 135 °C

With palladium diacetate; potassium carbonate; dicyclohexyl-carbodiimide; triphenylphosphine; In tetrahydrofuran; toluene;
DOI:10.1021/ja054558o