allylammonium tetraphenylborate

Base Information

Chemical Name:allylammonium tetraphenylborate
CAS No.:116506-06-0
Molecular Formula:C₃H₇N*C₂₄H₂₀B*H
Molecular Weight:377.337
Hs Code.:

Synonyms:allylammonium tetraphenylborate

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Chemical Property of allylammonium tetraphenylborate

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Technology Process of allylammonium tetraphenylborate

There total 1 articles about allylammonium tetraphenylborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 107-11-9,30551-89-4
1-amino-2-propene

: lithium tetraphenylborate tris(1,2-dimethoxyethane)

: 116506-06-0
allylammonium tetraphenylborate

Guidance literature:: 1-amino-2-propene; lithium tetraphenylborate tris(1,2-dimethoxyethane); With carbon dioxide; In tetrahydrofuran; at -0.16 ℃; Inert atmosphere;

In pentane; at -20.16 ℃; Inert atmosphere;
DOI:10.1021/om960602k

Reference yield: 80.0%

: 153698-14-7
[Pd(1,2-bis(diphenylphosphino)ethane)(dibenzylideneacetone)]

: 116506-06-0
allylammonium tetraphenylborate

: 497152-76-8
[η3-C3H5)Pd(1,2-bis(diphenylphosphino)ethane)][BPh4]

Guidance literature:: In tetrahydrofuran; byproducts: NH3, dibenzylideneacetone; under N2; BPh4-contg. compd. (0.145 mmol) was added to a THF soln. of Pd-contg. compd. (0.144 mmol); stirring at 293 K for 2 h; the mixt. was concd. in vac.; Et2O was added; cooling to 253 K overnight; the oil was isolated by removing the mother soln. and washed with Et2O; drying in vac.; elem. anal.;
DOI:10.1016/S0022-328X(02)01897-1

Reference yield: 75.0%

: [Ni(PCy₃)2]2(N₂)

: 116506-06-0
allylammonium tetraphenylborate

: 185697-00-1
[(η(3)-C3H5)Ni(PCy3)(NH3)]BPh4

Guidance literature:: In tetrahydrofuran; byproducts: PCy3, N2; to a soln. of complex in THF, prepared under N2 at 243 K, was added allylammoniumBPh4 in THF, the mixt. was stirred at room temp. (293 K) untilorange color (N2 atm.); filtered, concd. in vac., pentane was added, cooled to 253 K, crystals were washed with pentane, dried in vac.; elem. anal.;
DOI:10.1021/om000383+