C₅₇H₉₆N₄O₁₃SSi

Base Information

Chemical Name:C₅₇H₉₆N₄O₁₃SSi
CAS No.:582321-83-3
Molecular Formula:C₅₇H₉₆N₄O₁₃SSi
Molecular Weight:1105.56
Hs Code.:

C<sub>57</sub>H<sub>96</sub>N<sub>4</sub>O<sub>13</sub>SSi

Synonyms:C₅₇H₉₆N₄O₁₃SSi

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Chemical Property of C₅₇H₉₆N₄O₁₃SSi

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Technology Process of C₅₇H₉₆N₄O₁₃SSi

There total 22 articles about C₅₇H₉₆N₄O₁₃SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 582321-82-2
C₆₅H₁₀₄N₄O₁₄SSi

: 582321-83-3
C₅₇H₉₆N₄O₁₃SSi

Guidance literature:: With 2,6-dichloro-3,5-dicyano-1,4-benzoquinone; In phosphate buffer; dichloromethane; at 0 - 20 ℃; for 1.5h; pH=7;
DOI:10.1021/ja036050w

Reference yield:

: 15761-39-4,59433-50-0
1-(tert-butoxycarbonyl)-L-proline

: 582321-83-3
C₅₇H₉₆N₄O₁₃SSi

Guidance literature:: Multi-step reaction with 9 steps

1.1: diisopropylethylamine; 2,4,6-trichlorobenzoyl chloride / tetrahydrofuran / 3 h / 20 °C

1.2: 94 percent / N,N-dimethyl-4-aminopyridine / toluene / 3 h / 20 °C

2.1: 88 percent / tetra-N-butylammonium fluoride / tetrahydrofuran / 5 h / 20 °C

3.1: 4 Angstroem molecular sieves; N-methylmorpholine-N-oxide; tetra-n-propylammonium perruthenate / CH₂Cl₂ / 0.5 h / 20 °C

4.1: dicyclohexylboron chloride; Me₂NEt / diethyl ether / 1.5 h / 0 °C

4.2: diethyl ether / 19 h / -78 - -20 °C

4.3: aq. H₂O₂ / methanol / 3 h / 20 °C

5.1: 196 mg / 2,6-lutidine / CH₂Cl₂ / 2 h / -50 °C

6.1: K₂CO₃ / methanol / 2 h / 20 °C

7.1: 39.3 mg / aq. NaIO₄ / 2-methyl-propan-2-ol / 12 h / 20 °C

8.1: 75.5 mg / Et₃N; diphenylphosphoryl azide / dimethylformamide / 2 h / 20 °C

9.1: 93 percent / 2,6-dichloro-3,5-dicyanoquinone / CH₂Cl₂; aq. phosphate buffer / 1.5 h / 0 - 20 °C / pH 7

With 2,6-dimethylpyridine; sodium periodate; tetrapropylammonium perruthennate; N,N-dimethyl-ethanamine; 4 A molecular sieve; 2,4,6-trichlorobenzoyl chloride; diphenylphosphoranyl azide; dicyclohexylboron chloride; tetrabutyl ammonium fluoride; 2,6-dichloro-3,5-dicyano-1,4-benzoquinone; potassium carbonate; 4-methylmorpholine N-oxide; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; phosphate buffer; diethyl ether; dichloromethane; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1021/ja036050w

Reference yield:

: 67760-86-5
(3S)-2,2-dimethyl-5-hexen-3-ol

: 582321-83-3
C₅₇H₉₆N₄O₁₃SSi

Guidance literature:: Multi-step reaction with 14 steps

1.1: 71 percent / Et₃N; N-methyl-2-chloropyridinium iodide / CH₂Cl₂ / 2.5 h / Heating

2.1: titanium tetra-isopropoxide / CH₂Cl₂ / 1 h / 40 °C

2.2: 97 percent / benzylidene-bis(tricyclohexylphosphine)dichlororuthenium / CH₂Cl₂ / 3 h / Heating

3.1: CuCN / diethyl ether / -78 - 0 °C

3.2: 86 percent / diethyl ether / 1 h / -78 - -25 °C

4.1: 83 percent / LiAlH₄ / diethyl ether / 0.67 h / 0 °C

5.1: 86 percent / imidazole / CH₂Cl₂ / 0.5 h / 20 °C

6.1: diisopropylethylamine; 2,4,6-trichlorobenzoyl chloride / tetrahydrofuran / 3 h / 20 °C

6.2: 94 percent / N,N-dimethyl-4-aminopyridine / toluene / 3 h / 20 °C

7.1: 88 percent / tetra-N-butylammonium fluoride / tetrahydrofuran / 5 h / 20 °C

8.1: 4 Angstroem molecular sieves; N-methylmorpholine-N-oxide; tetra-n-propylammonium perruthenate / CH₂Cl₂ / 0.5 h / 20 °C

9.1: dicyclohexylboron chloride; Me₂NEt / diethyl ether / 1.5 h / 0 °C

9.2: diethyl ether / 19 h / -78 - -20 °C

9.3: aq. H₂O₂ / methanol / 3 h / 20 °C

10.1: 196 mg / 2,6-lutidine / CH₂Cl₂ / 2 h / -50 °C

11.1: K₂CO₃ / methanol / 2 h / 20 °C

12.1: 39.3 mg / aq. NaIO₄ / 2-methyl-propan-2-ol / 12 h / 20 °C

13.1: 75.5 mg / Et₃N; diphenylphosphoryl azide / dimethylformamide / 2 h / 20 °C

14.1: 93 percent / 2,6-dichloro-3,5-dicyanoquinone / CH₂Cl₂; aq. phosphate buffer / 1.5 h / 0 - 20 °C / pH 7

With 1H-imidazole; 2,6-dimethylpyridine; titanium(IV) isopropylate; sodium periodate; lithium aluminium tetrahydride; tetrapropylammonium perruthennate; N,N-dimethyl-ethanamine; 4 A molecular sieve; 2,4,6-trichlorobenzoyl chloride; diphenylphosphoranyl azide; dicyclohexylboron chloride; tetrabutyl ammonium fluoride; 2-chloro-1-methyl-pyridinium iodide; 2,6-dichloro-3,5-dicyano-1,4-benzoquinone; potassium carbonate; 4-methylmorpholine N-oxide; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; phosphate buffer; diethyl ether; dichloromethane; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1021/ja036050w