C₃₄H₃₄N₂O₁₀

Base Information

Chemical Name:C₃₄H₃₄N₂O₁₀
CAS No.:1280608-68-5
Molecular Formula:C₃₄H₃₄N₂O₁₀
Molecular Weight:630.651
Hs Code.:

C<sub>34</sub>H<sub>34</sub>N<sub>2</sub>O<sub>10</sub>

Synonyms:C₃₄H₃₄N₂O₁₀

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Chemical Property of C₃₄H₃₄N₂O₁₀

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Technology Process of C₃₄H₃₄N₂O₁₀

There total 12 articles about C₃₄H₃₄N₂O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1280608-87-8
C₃₄H₃₆N₂O₁₀

: 1280608-68-5
C₃₄H₃₄N₂O₁₀

Guidance literature:: With Dess-Martin periodane; In dichloromethane; at 0 - 20 ℃;
DOI:10.1002/anie.201006528

Reference yield:

: 1280608-57-2
C₃₀H₃₅NO₉

: 1280608-68-5
C₃₄H₃₄N₂O₁₀

Guidance literature:: Multi-step reaction with 6 steps

1.1: 2,6-dimethylpyridine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

2.1: pyridine; pyridine hydrofluoride / tetrahydrofuran / 8 h / -78 - 0 °C

3.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 0 - 20 °C

4.1: n-butyllithium / tetrahydrofuran; hexane / -78 °C / Inert atmosphere

4.2: -78 °C / Inert atmosphere

5.1: toluene-4-sulfonic acid / tetrahydrofuran; water / 4.5 h / Reflux

6.1: Dess-Martin periodane / dichloromethane / 0 - 20 °C

With pyridine; 2,6-dimethylpyridine; n-butyllithium; pyridine hydrofluoride; sodium hydrogencarbonate; Dess-Martin periodane; toluene-4-sulfonic acid; In tetrahydrofuran; hexane; dichloromethane; water; 3.1: Dess-Martin oxidation / 6.1: Dess-Martin oxidation;
DOI:10.1002/anie.201006528

Reference yield:

: 1280608-40-3
C₂₃H₂₅NO₆

: 1280608-68-5
C₃₄H₃₄N₂O₁₀

Guidance literature:: Multi-step reaction with 11 steps

1.1: sodium tetrahydroborate / tetrahydrofuran; methanol / 0 °C

2.1: sodium hydride / tetrahydrofuran; mineral oil / 0 °C

2.2: 2.5 h / 20 °C

3.1: Oxone; C₁₃H₂₀O₉; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate / Dimethoxymethane; water; acetonitrile / 24 h / 0 °C / pH 6 / aq. phosphate buffer

4.1: water; pyridinium p-toluenesulfonate / 1,4-dioxane / 12 h / 70 °C

5.1: [bis(acetoxy)iodo]benzene; potassium hydroxide / 2 h / 0 °C

6.1: 2,6-dimethylpyridine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

7.1: pyridine; pyridine hydrofluoride / tetrahydrofuran / 8 h / -78 - 0 °C

8.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 0 - 20 °C

9.1: n-butyllithium / tetrahydrofuran; hexane / -78 °C / Inert atmosphere

9.2: -78 °C / Inert atmosphere

10.1: toluene-4-sulfonic acid / tetrahydrofuran; water / 4.5 h / Reflux

11.1: Dess-Martin periodane / dichloromethane / 0 - 20 °C

With pyridine; 2,6-dimethylpyridine; Oxone; sodium tetrahydroborate; n-butyllithium; C₁₃H₂₀O₉; pyridine hydrofluoride; [bis(acetoxy)iodo]benzene; water; tetra(n-butyl)ammonium hydrogensulfate; pyridinium p-toluenesulfonate; sodium hydride; sodium hydrogencarbonate; potassium carbonate; Dess-Martin periodane; toluene-4-sulfonic acid; potassium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; Dimethoxymethane; hexane; dichloromethane; water; acetonitrile; mineral oil; 3.1: Shi epoxidation / 8.1: Dess-Martin oxidation / 11.1: Dess-Martin oxidation;
DOI:10.1002/anie.201006528