(3S,6S,7S)-7-(tert-butyldimethylsilyloxy)-6-(4-methoxybenzyloxy)-3-methylundec-10-enal

Base Information

Chemical Name:(3S,6S,7S)-7-(tert-butyldimethylsilyloxy)-6-(4-methoxybenzyloxy)-3-methylundec-10-enal
CAS No.:1173997-16-4
Molecular Formula:C₂₆H₄₄O₄Si
Molecular Weight:448.718
Hs Code.:

Synonyms:(3S,6S,7S)-7-(tert-butyldimethylsilyloxy)-6-(4-methoxybenzyloxy)-3-methylundec-10-enal

Suppliers and Price of (3S,6S,7S)-7-(tert-butyldimethylsilyloxy)-6-(4-methoxybenzyloxy)-3-methylundec-10-enal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3S,6S,7S)-7-(tert-butyldimethylsilyloxy)-6-(4-methoxybenzyloxy)-3-methylundec-10-enal

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Technology Process of (3S,6S,7S)-7-(tert-butyldimethylsilyloxy)-6-(4-methoxybenzyloxy)-3-methylundec-10-enal

There total 1 articles about (3S,6S,7S)-7-(tert-butyldimethylsilyloxy)-6-(4-methoxybenzyloxy)-3-methylundec-10-enal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1173997-15-3
(3S,6S,7S)-7-(tert-butyldimethylsilyloxy)-6-(4-methoxybenzyloxy)-3-methylundec-10-en-1-ol

: 1173997-16-4
(3S,6S,7S)-7-(tert-butyldimethylsilyloxy)-6-(4-methoxybenzyloxy)-3-methylundec-10-enal

Guidance literature:: With Dess-Martin periodane; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ol900936t

Reference yield: 84.0%

: 1173997-16-4
(3S,6S,7S)-7-(tert-butyldimethylsilyloxy)-6-(4-methoxybenzyloxy)-3-methylundec-10-enal

: 263764-23-4,863324-53-2
(S)-3-propanoyl-4-benzyl-1,3-thiazolidine-2-thione

: (5S,8S,9S)-1-[(4S)-4-benzyl-2-thioxothiazolidin-3-yl]-9-(tert-butyldimethylsilyloxy)-3-hydroxy-8-(4-methoxybenzyloxy)-2,5-dimethyltridec-12-en-1-one

Guidance literature:: (S)-3-propanoyl-4-benzyl-1,3-thiazolidine-2-thione; With titanium tetrachloride; In dichloromethane; at 0 ℃; for 0.166667h; Inert atmosphere;

With sparteine; In dichloromethane; at 0 ℃; for 0.666667h; Inert atmosphere;

(3S,6S,7S)-7-(tert-butyldimethylsilyloxy)-6-(4-methoxybenzyloxy)-3-methylundec-10-enal; With 1-methyl-pyrrolidin-2-one; In dichloromethane; at 0 ℃; for 0.5h; optical yield given as %de; Inert atmosphere;
DOI:10.1021/ol900936t