Technology Process of C35H35N3O9S
There total 7 articles about C35H35N3O9S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
methylthioacetic acid ethyl ester; C32H33N3O8;
With
sulfuryl dichloride;
In
dichloromethane;
at -78 - 20 ℃;
With
acetic acid; triethylamine;
at 20 ℃;
for 1h;
DOI:10.1002/ejoc.201001629
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: trifluorormethanesulfonic acid / dichloromethane / 2 h / -78 - 0 °C
2.1: triethylamine / dichloromethane / 1 h / 23 °C
3.1: 1,1'-bis-(diphenylphosphino)ferrocene; formic acid; tributylsilane; palladium diacetate; triethylamine / N,N-dimethyl-formamide / 1 h / 50 °C
4.1: sulfuryl dichloride / dichloromethane / -78 - 20 °C
4.2: 1 h / 20 °C
With
1,1'-bis-(diphenylphosphino)ferrocene; formic acid; sulfuryl dichloride; tributylsilane; trifluorormethanesulfonic acid; palladium diacetate; triethylamine;
In
dichloromethane; N,N-dimethyl-formamide;
3.1: Gassman synthesis;
DOI:10.1002/ejoc.201001629
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: 1,1'-bis-(diphenylphosphino)ferrocene; formic acid; tributylsilane; palladium diacetate; triethylamine / N,N-dimethyl-formamide / 1 h / 50 °C
2.1: sulfuryl dichloride / dichloromethane / -78 - 20 °C
2.2: 1 h / 20 °C
With
1,1'-bis-(diphenylphosphino)ferrocene; formic acid; sulfuryl dichloride; tributylsilane; palladium diacetate; triethylamine;
In
dichloromethane; N,N-dimethyl-formamide;
1.1: Gassman synthesis;
DOI:10.1002/ejoc.201001629
