Technology Process of C28H35NO5S
There total 3 articles about C28H35NO5S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C23H31NO4; p-toluenesulfonyl chloride;
With
sodium hydride;
In
tetrahydrofuran;
at 0 - 20 ℃;
for 0.166667h;
With
diisobutylaluminium hydride;
In
tetrahydrofuran;
at 0 ℃;
for 0.5h;
DOI:10.1016/j.bmc.2014.02.043
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: N-ethyl-N,N-diisopropylamine; tetra-(n-butyl)ammonium iodide; zinc trifluoromethanesulfonate / toluene / 0.25 h / 20 °C
1.2: 3 h
2.1: sodium hydride / tetrahydrofuran / 0.17 h / 0 - 20 °C
2.2: 0.5 h / 0 °C
With
tetra-(n-butyl)ammonium iodide; zinc trifluoromethanesulfonate; sodium hydride; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; toluene;
DOI:10.1016/j.bmc.2014.02.043
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: N-ethyl-N,N-diisopropylamine; tetra-(n-butyl)ammonium iodide; zinc trifluoromethanesulfonate / toluene / 0.25 h / 20 °C
1.2: 3 h
2.1: sodium hydride / tetrahydrofuran / 0.17 h / 0 - 20 °C
2.2: 0.5 h / 0 °C
With
tetra-(n-butyl)ammonium iodide; zinc trifluoromethanesulfonate; sodium hydride; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; toluene;
DOI:10.1016/j.bmc.2014.02.043