C₂₅H₃₄O₇

Base Information

• Chemical Name: C₂₅H₃₄O₇
• CAS No.: 391278-04-9
• Molecular Formula: C₂₅H₃₄O₇
• Molecular Weight: 446.541
• Mol file: 391278-04-9.mol

Synonyms:C₂₅H₃₄O₇

Chemical Property of C₂₅H₃₄O₇

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₅H₃₄O₇

There total 21 articles about C₂₅H₃₄O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

C32H40O7 (391278-03-8) → C18H28O7 (790664-57-2) + C25H34O7 (391278-04-9)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethyl acetate;

DOI:10.1016/j.tet.2004.07.094

Reference yield: 70.0%

C32H40O7 (391278-03-8) → C25H34O7 (391278-04-9)

Guidance literature:

With hydrogen; palladium on activated charcoal;

DOI:10.1016/S0040-4039(01)01802-0

Reference yield:

C16H26O6 (391277-97-7) → C25H34O7 (391278-04-9)

Guidance literature:

Multi-step reaction with 9 steps

1.1: 92 percent / p-TsOH / CH₂Cl₂ / 24 h / 20 °C

2.1: K₂CO₃ / methanol / 4 h / 20 °C

2.2: 90 percent / PCC / CH₂Cl₂ / 3 h / 20 °C

3.1: 88 percent / Et₃N / CH₂Cl₂ / 0.5 h / -78 °C

4.1: 73 percent / Na₂(EDTA); oxone; NaHCO₃ / H₂O; acetone; acetonitrile / 4 h / 20 °C

5.1: 79 percent / Al(OiPr)3 / toluene / 1 h / 20 °C

6.1: Me₃SiCl; Et₃N; DMAP / CH₂Cl₂ / 0.33 h / 20 °C

6.2: tetrahydrofuran / 0.17 h / -78 °C

6.3: 90 percent / HCl / tetrahydrofuran; H₂O / 0.5 h / 20 °C

7.1: NaH / tetrahydrofuran / 0 - 20 °C

7.2: 86 percent / tetrahydrofuran / 12 h / Heating

8.1: OsO₄; N-methylmorpholine-N-oxide / acetone; H₂O / 96 h / 20 °C

8.2: 78 percent / NaIO₄ / acetone; H₂O / 48 h / 20 °C

9.1: 70 percent / H₂ / Pd/C / ethyl acetate

With dmap; Oxone; osmium(VIII) oxide; chloro-trimethyl-silane; hydrogen; edetate disodium; aluminum isopropoxide; sodium hydride; sodium hydrogencarbonate; potassium carbonate; toluene-4-sulfonic acid; 4-methylmorpholine N-oxide; triethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; acetone; toluene; acetonitrile;

DOI:10.1016/j.tet.2004.07.094

upstream raw materials:

C₃₂H₄₀O₇

(S)-p-mentha-6,8-dien-2-one

C₁₇H₂₆O₅

C₁₆H₂₆O₆

Downstream raw materials:

C₂₅H₃₄O₆

C₂₆H₃₈O₉S

C₂₅H₃₆O₇