p-trifluoroacetamidophenyl 4-O-(2,4-di-O-benzyl-3,6-di-O-methyl-β-D-glucopyranosyl)-2,3-di-O-methyl-α-L-rhamnopyranoside

Base Information

Chemical Name:p-trifluoroacetamidophenyl 4-O-(2,4-di-O-benzyl-3,6-di-O-methyl-β-D-glucopyranosyl)-2,3-di-O-methyl-α-L-rhamnopyranoside
CAS No.:150412-62-7
Molecular Formula:C₃₈H₄₆F₃NO₁₁
Molecular Weight:749.779
Hs Code.:

Synonyms:p-trifluoroacetamidophenyl 4-O-(2,4-di-O-benzyl-3,6-di-O-methyl-β-D-glucopyranosyl)-2,3-di-O-methyl-α-L-rhamnopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of p-trifluoroacetamidophenyl 4-O-(2,4-di-O-benzyl-3,6-di-O-methyl-β-D-glucopyranosyl)-2,3-di-O-methyl-α-L-rhamnopyranoside

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Technology Process of p-trifluoroacetamidophenyl 4-O-(2,4-di-O-benzyl-3,6-di-O-methyl-β-D-glucopyranosyl)-2,3-di-O-methyl-α-L-rhamnopyranoside

There total 2 articles about p-trifluoroacetamidophenyl 4-O-(2,4-di-O-benzyl-3,6-di-O-methyl-β-D-glucopyranosyl)-2,3-di-O-methyl-α-L-rhamnopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 2709-93-5
N-trifluoroacetyl-4-aminophenol

: 150412-61-6
ethyl 4-O-(2,4-di-O-benzyl-3,6-di-O-methyl-β-D-glucopyranosyl)-2,3-di-O-methyl-1-thio-α-L-rhamnopyranoside

: 150412-62-7
p-trifluoroacetamidophenyl 4-O-(2,4-di-O-benzyl-3,6-di-O-methyl-β-D-glucopyranosyl)-2,3-di-O-methyl-α-L-rhamnopyranoside

Guidance literature:: With 4 A molecular sieve; methyl trifluoromethanesulfonate; In dichloromethane; for 5h;
DOI:10.1016/0008-6215(93)80099-Z

Reference yield:

: 123-30-8
4-amino-phenol

: 150412-62-7
p-trifluoroacetamidophenyl 4-O-(2,4-di-O-benzyl-3,6-di-O-methyl-β-D-glucopyranosyl)-2,3-di-O-methyl-α-L-rhamnopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / 1 h

2: 84 percent / methyl triflate, molecular sieves 4 Angstroem / CH₂Cl₂ / 5 h

With 4 A molecular sieve; methyl trifluoromethanesulfonate; In dichloromethane; trifluoroacetic acid;
DOI:10.1016/0008-6215(93)80099-Z

Reference yield: 92.0%

: 150412-62-7
p-trifluoroacetamidophenyl 4-O-(2,4-di-O-benzyl-3,6-di-O-methyl-β-D-glucopyranosyl)-2,3-di-O-methyl-α-L-rhamnopyranoside

: p-trifluoroacetamidophenyl 4-O-(3,6-di-O-methyl-β-D-glucopyranosyl)-2,3-di-O-methyl-α-L-rhamnopyranoside

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; for 10h; Ambient temperature;
DOI:10.1016/0008-6215(93)80099-Z