4-methoxyphenyl (sodium 5-acetamido-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonate)-(2->6)-(β-D-galactopyranosyl)-(1->6)-(β-D-glucopyranosyl)-(1->3)-(β-D-galactopyranosyl)-(1->3)-2-acetamido-2-deoxy-β-D-galactopyranoside

Base Information

• Chemical Name: 4-methoxyphenyl (sodium 5-acetamido-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonate)-(2->6)-(β-D-galactopyranosyl)-(1->6)-(β-D-glucopyranosyl)-(1->3)-(β-D-galactopyranosyl)-(1->3)-2-acetamido-2-deoxy-β-D-galactopyranoside
• CAS No.: 1221254-70-1
• Molecular Formula: C₄₄H₆₇N₂O₃₀*Na
• Molecular Weight: 1127

Synonyms:4-methoxyphenyl (sodium 5-acetamido-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonate)-(2->6)-(β-D-galactopyranosyl)-(1->6)-(β-D-glucopyranosyl)-(1->3)-(β-D-galactopyranosyl)-(1->3)-2-acetamido-2-deoxy-β-D-galactopyranoside

Chemical Property of 4-methoxyphenyl (sodium 5-acetamido-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonate)-(2->6)-(β-D-galactopyranosyl)-(1->6)-(β-D-glucopyranosyl)-(1->3)-(β-D-galactopyranosyl)-(1->3)-2-acetamido-2-deoxy-β-D-galactopyranoside

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Technology Process of 4-methoxyphenyl (sodium 5-acetamido-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonate)-(2->6)-(β-D-galactopyranosyl)-(1->6)-(β-D-glucopyranosyl)-(1->3)-(β-D-galactopyranosyl)-(1->3)-2-acetamido-2-deoxy-β-D-galactopyranoside

There total 1 articles about 4-methoxyphenyl (sodium 5-acetamido-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonate)-(2->6)-(β-D-galactopyranosyl)-(1->6)-(β-D-glucopyranosyl)-(1->3)-(β-D-galactopyranosyl)-(1->3)-2-acetamido-2-deoxy-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

4-methoxyphenyl (methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonate)-(2->6)-(2,3,4-tri-O-acetyl-β-D-galactopyranosyl-(1->6)-2,3,4-tri-O-acetyl-β-D-glucopyranosyl)-(1->3)-(2-O-acetyl-4,6-O-benzylidene-β-D-galactopyranosyl)-(1->3)-2-acetamido-4,6-O-benzylidene-2-deoxy-β-D-galactopyranoside → 4-methoxyphenyl (sodium 5-acetamido-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonate)-(2->6)-(β-D-galactopyranosyl)-(1->6)-(β-D-glucopyranosyl)-(1->3)-(β-D-galactopyranosyl)-(1->3)-2-acetamido-2-deoxy-β-D-galactopyranoside (1221254-70-1)

Guidance literature:

4-methoxyphenyl (methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonate)-(2->6)-(2,3,4-tri-O-acetyl-β-D-galactopyranosyl-(1->6)-2,3,4-tri-O-acetyl-β-D-glucopyranosyl)-(1->3)-(2-O-acetyl-4,6-O-benzylidene-β-D-galactopyranosyl)-(1->3)-2-acetamido-4,6-O-benzylidene-2-deoxy-β-D-galactopyranoside; With Pearlman's catalist; hydrogen; In methanol; at 20 ℃; for 24h;

With methanol; sodium methylate; at 20 ℃; for 12h; Further stages;

DOI:10.1016/j.bioorg.2010.01.001

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