5,15-diphenyl-2,8,12,18-tetra(n-hexyl)-3,7,13,17-tetramethylporphyrin zinc(II)

Base Information

Chemical Name:5,15-diphenyl-2,8,12,18-tetra(n-hexyl)-3,7,13,17-tetramethylporphyrin zinc(II)
CAS No.:244301-43-7
Molecular Formula:C₆₀H₇₆N₄Zn
Molecular Weight:918.68
Hs Code.:

Synonyms:5,15-diphenyl-2,8,12,18-tetra(n-hexyl)-3,7,13,17-tetramethylporphyrin zinc(II)

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Chemical Property of 5,15-diphenyl-2,8,12,18-tetra(n-hexyl)-3,7,13,17-tetramethylporphyrin zinc(II)

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Technology Process of 5,15-diphenyl-2,8,12,18-tetra(n-hexyl)-3,7,13,17-tetramethylporphyrin zinc(II)

There total 2 articles about 5,15-diphenyl-2,8,12,18-tetra(n-hexyl)-3,7,13,17-tetramethylporphyrin zinc(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: H₂ 5,15-bis(phenyl)-2,8,12,18-tetrahexyl-3,7,13,17-tetramethylporphyrin

: 244301-43-7
5,15-diphenyl-2,8,12,18-tetra(n-hexyl)-3,7,13,17-tetramethylporphyrin zinc(II)

Guidance literature:: With zinc(II) acetate dihydrate; In methanol; chloroform; for 0.333333h; Reflux;
DOI:10.1039/c1dt10880h

Reference yield:

: (C₄NCC₆H₁₃CH₃)4H₄(C₆H₅)2

: 5970-45-6
zinc(II) acetate dihydrate

: 244301-43-7
5,15-diphenyl-2,8,12,18-tetra(n-hexyl)-3,7,13,17-tetramethylporphyrin zinc(II)

Guidance literature:: In methanol; chloroform; excess of Zn-contg. compd. (ca. 5 equivs.) was added to a stirred soln. of the ligand (1 equiv.) in CHCl3-MeOH soln. (10% MeOH); the mixt. was refluxed for 20 min; the soln. was washed with H2O2, dried over Na2SO4, filtered and passed through a plug of silica gel; the solvent was removed under reduced pressure; column chromy. over silica gel; recrystn. using combination of solvents;
DOI:10.1039/c1dt10880h