Technology Process of C20H24OS2
There total 5 articles about C20H24OS2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium tetrahydroborate;
In
methanol;
at 0 ℃;
for 0.5h;
Sealed tube;
DOI:10.1055/s-0032-1318220
- Guidance literature:
-
Multi-step reaction with 3 steps
1: diisobutylaluminium hydride / tetrahydrofuran; toluene / 1 h / -40 °C / Sealed tube
2: C13H18N2O*C7H6O2; sodium dihydrogenphosphate / acetonitrile; water / 24 h / 0 °C / Sealed tube
3: sodium tetrahydroborate / methanol / 0.5 h / 0 °C / Sealed tube
With
sodium tetrahydroborate; sodium dihydrogenphosphate; C13H18N2O*C7H6O2; diisobutylaluminium hydride;
In
tetrahydrofuran; methanol; water; toluene; acetonitrile;
DOI:10.1055/s-0032-1318220
- Guidance literature:
-
Multi-step reaction with 5 steps
1: dichloromethane / 20 °C / Sealed tube
2: palladium 10% on activated carbon; hydrogen / methanol / 3 h / 760.05 Torr / Sealed tube
3: diisobutylaluminium hydride / tetrahydrofuran; toluene / 1 h / -40 °C / Sealed tube
4: C13H18N2O*C7H6O2; sodium dihydrogenphosphate / acetonitrile; water / 24 h / 0 °C / Sealed tube
5: sodium tetrahydroborate / methanol / 0.5 h / 0 °C / Sealed tube
With
sodium tetrahydroborate; sodium dihydrogenphosphate; palladium 10% on activated carbon; C13H18N2O*C7H6O2; hydrogen; diisobutylaluminium hydride;
In
tetrahydrofuran; methanol; dichloromethane; water; toluene; acetonitrile;
DOI:10.1055/s-0032-1318220
