(R)-(Z)-N-methyl-N-<2-(2-(2'-(p-tolylsulfinyl)-1'-ethenyl)-4,5-dimethoxyphenyl)ethyl>trifluoroacetamide

Base Information

Chemical Name:(R)-(Z)-N-methyl-N-<2-(2-(2'-(p-tolylsulfinyl)-1'-ethenyl)-4,5-dimethoxyphenyl)ethyl>trifluoroacetamide
CAS No.:109985-73-1
Molecular Formula:C₂₂H₂₄F₃NO₄S
Molecular Weight:455.498
Hs Code.:

Synonyms:(R)-(Z)-N-methyl-N-<2-(2-(2'-(p-tolylsulfinyl)-1'-ethenyl)-4,5-dimethoxyphenyl)ethyl>trifluoroacetamide

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Chemical Property of (R)-(Z)-N-methyl-N-<2-(2-(2'-(p-tolylsulfinyl)-1'-ethenyl)-4,5-dimethoxyphenyl)ethyl>trifluoroacetamide

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Technology Process of (R)-(Z)-N-methyl-N-<2-(2-(2'-(p-tolylsulfinyl)-1'-ethenyl)-4,5-dimethoxyphenyl)ethyl>trifluoroacetamide

There total 4 articles about (R)-(Z)-N-methyl-N-<2-(2-(2'-(p-tolylsulfinyl)-1'-ethenyl)-4,5-dimethoxyphenyl)ethyl>trifluoroacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 110527-65-6
N-methyl-N-(2-(3',4'-dimethoxyphenyl)ethyl)trifluoroacetamide

: 109985-73-1
(R)-(Z)-N-methyl-N-<2-(2-(2'-(p-tolylsulfinyl)-1'-ethenyl)-4,5-dimethoxyphenyl)ethyl>trifluoroacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 40 percent / trifluoroacetic acid / 12 h / Heating

2: 1.) BuLi / 1.) DMSO, -78 deg C, 1h, 2.) -78 deg C, 30 min

With n-butyllithium; In trifluoroacetic acid;
DOI:10.1021/jo00290a051

Reference yield:

: 120-20-7
2-(3,4-dimethoxyphenyl)-ethylamine

: 109985-73-1
(R)-(Z)-N-methyl-N-<2-(2-(2'-(p-tolylsulfinyl)-1'-ethenyl)-4,5-dimethoxyphenyl)ethyl>trifluoroacetamide

Guidance literature:: Multi-step reaction with 3 steps

1: 2)KOH / 1)pyridine, 2)acetone

2: 40 percent / trifluoroacetic acid / 12 h / Heating

3: 1.) BuLi / 1.) DMSO, -78 deg C, 1h, 2.) -78 deg C, 30 min

With potassium hydroxide; n-butyllithium; In trifluoroacetic acid;
DOI:10.1021/jo00290a051

Reference yield:

: 61187-71-1
(+)-(R)-(dimethoxyphosphoryl)methyl p-tolyl sulfoxide

: 109985-71-9
N-methyl-N-(2-(2'-formyl-4',5'-dimethoxyphenyl)ethyl)trifluoroacetamide

: 109985-73-1
(R)-(Z)-N-methyl-N-<2-(2-(2'-(p-tolylsulfinyl)-1'-ethenyl)-4,5-dimethoxyphenyl)ethyl>trifluoroacetamide

: 109985-72-0
(R)-(E)-N-methyl-N-<2-(2-(2'-(p-tolylsulfinyl)-1'-ethenyl)-4,5-dimethoxyphenyl)ethyl>trifluoroacetamide

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction; 1.) THF, -78 deg, 1h, 2.) -78 deg C, 30 min;
DOI:10.1021/jo00290a051