(S)-1-((2S,3R)-2-Amino-3-benzyloxy-butyryl)-pyrrolidine-2-carboxylic acid amide; hydrochloride

Base Information

Chemical Name:(S)-1-((2S,3R)-2-Amino-3-benzyloxy-butyryl)-pyrrolidine-2-carboxylic acid amide; hydrochloride
CAS No.:78058-22-7
Molecular Formula:C₁₆H₂₃N₃O₃*ClH
Molecular Weight:341.838
Hs Code.:

Synonyms:(S)-1-((2S,3R)-2-Amino-3-benzyloxy-butyryl)-pyrrolidine-2-carboxylic acid amide; hydrochloride

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Chemical Property of (S)-1-((2S,3R)-2-Amino-3-benzyloxy-butyryl)-pyrrolidine-2-carboxylic acid amide; hydrochloride

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Technology Process of (S)-1-((2S,3R)-2-Amino-3-benzyloxy-butyryl)-pyrrolidine-2-carboxylic acid amide; hydrochloride

There total 3 articles about (S)-1-((2S,3R)-2-Amino-3-benzyloxy-butyryl)-pyrrolidine-2-carboxylic acid amide; hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 61884-24-0
[(1S,2R)-2-Benzyloxy-1-((S)-2-carbamoyl-pyrrolidine-1-carbonyl)-propyl]-carbamic acid tert-butyl ester

: 78058-22-7
(S)-1-((2S,3R)-2-Amino-3-benzyloxy-butyryl)-pyrrolidine-2-carboxylic acid amide; hydrochloride

Guidance literature:: With hydrogenchloride; In ethyl acetate; for 1h; Ambient temperature;
DOI:10.1021/jm00372a006

Reference yield:

: 70989-89-8
Boc-Thr(Bzl)-OPfp

: 78058-22-7
(S)-1-((2S,3R)-2-Amino-3-benzyloxy-butyryl)-pyrrolidine-2-carboxylic acid amide; hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: DMFA / 1 h / Ambient temperature

2: 2 N HCl / ethyl acetate / 1 h / Ambient temperature

With hydrogenchloride; N,N-dimethyl-formamide; In ethyl acetate;
DOI:10.1021/jm00372a006

Reference yield:

: 7531-52-4
L-prolinamide

: 78058-22-7
(S)-1-((2S,3R)-2-Amino-3-benzyloxy-butyryl)-pyrrolidine-2-carboxylic acid amide; hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: DMFA / 1 h / Ambient temperature

2: 2 N HCl / ethyl acetate / 1 h / Ambient temperature

With hydrogenchloride; N,N-dimethyl-formamide; In ethyl acetate;
DOI:10.1021/jm00372a006