2-cyclobutyloxy-3-methyl-N-[2-(1H-tetrazol-5-yl)-indan-2-yl]-benzamide

Base Information

Chemical Name:2-cyclobutyloxy-3-methyl-N-[2-(1H-tetrazol-5-yl)-indan-2-yl]-benzamide
CAS No.:1092446-09-7
Molecular Formula:C₂₂H₂₃N₅O₂
Molecular Weight:389.457
Hs Code.:

Synonyms:2-cyclobutyloxy-3-methyl-N-[2-(1H-tetrazol-5-yl)-indan-2-yl]-benzamide

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Chemical Property of 2-cyclobutyloxy-3-methyl-N-[2-(1H-tetrazol-5-yl)-indan-2-yl]-benzamide

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Technology Process of 2-cyclobutyloxy-3-methyl-N-[2-(1H-tetrazol-5-yl)-indan-2-yl]-benzamide

There total 4 articles about 2-cyclobutyloxy-3-methyl-N-[2-(1H-tetrazol-5-yl)-indan-2-yl]-benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1092448-70-8
N-(2-cyano-indan-2-yl)-2-cyclobutyloxy-3-methyl-benzamide

: 1092446-09-7
2-cyclobutyloxy-3-methyl-N-[2-(1H-tetrazol-5-yl)-indan-2-yl]-benzamide

Guidance literature:: With trimethylsilylazide; di(n-butyl)tin oxide; In tetrahydrofuran; at 150 ℃; for 0.338889h; Microwave irradiation;

Reference yield:

: 23287-26-5
3-methylsalicylic acid methyl ester

: 1092446-09-7
2-cyclobutyloxy-3-methyl-N-[2-(1H-tetrazol-5-yl)-indan-2-yl]-benzamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: caesium carbonate / potassium iodide / N,N-dimethyl-formamide / 96 h / 43 °C

2.1: methanol; lithium hydroxide; water / 1,4-dioxane / 18 h

2.2: pH 2

3.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / dichloromethane / 0.08 h

3.2: 38 h

4.1: trimethylsilylazide; di(n-butyl)tin oxide / tetrahydrofuran / 0.34 h / 150 °C / Microwave irradiation

With methanol; lithium hydroxide; trimethylsilylazide; water; di(n-butyl)tin oxide; caesium carbonate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; potassium iodide; In tetrahydrofuran; 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 1092447-97-6
C₁₃H₁₆O₃

: 1092446-09-7
2-cyclobutyloxy-3-methyl-N-[2-(1H-tetrazol-5-yl)-indan-2-yl]-benzamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: methanol; lithium hydroxide; water / 1,4-dioxane / 18 h

1.2: pH 2

2.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / dichloromethane / 0.08 h

2.2: 38 h

3.1: trimethylsilylazide; di(n-butyl)tin oxide / tetrahydrofuran / 0.34 h / 150 °C / Microwave irradiation

With methanol; lithium hydroxide; trimethylsilylazide; water; di(n-butyl)tin oxide; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; In tetrahydrofuran; 1,4-dioxane; dichloromethane;