1-(3-chloro-4-fluorophenyl)-N-(3-chlorophenyl)-5-methyl-1H-1,2,3-triazole-4-carbothiamide

Base Information

Chemical Name:1-(3-chloro-4-fluorophenyl)-N-(3-chlorophenyl)-5-methyl-1H-1,2,3-triazole-4-carbothiamide
CAS No.:1187324-84-0
Molecular Formula:C₁₆H₁₁Cl₂FN₄S
Molecular Weight:381.261
Hs Code.:

Synonyms:1-(3-chloro-4-fluorophenyl)-N-(3-chlorophenyl)-5-methyl-1H-1,2,3-triazole-4-carbothiamide

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Chemical Property of 1-(3-chloro-4-fluorophenyl)-N-(3-chlorophenyl)-5-methyl-1H-1,2,3-triazole-4-carbothiamide

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Technology Process of 1-(3-chloro-4-fluorophenyl)-N-(3-chlorophenyl)-5-methyl-1H-1,2,3-triazole-4-carbothiamide

There total 5 articles about 1-(3-chloro-4-fluorophenyl)-N-(3-chlorophenyl)-5-methyl-1H-1,2,3-triazole-4-carbothiamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.6%

: 1187324-83-9
1-(3-chloro-4-fluorophenyl)-N-(3-chlorophenyl)-5-methyl-1H-1,2,3-triazole-4-carboxamide

: 1187324-84-0
1-(3-chloro-4-fluorophenyl)-N-(3-chlorophenyl)-5-methyl-1H-1,2,3-triazole-4-carbothiamide

Guidance literature:: With Lawessons reagent; In toluene; at 120 ℃; Microwave irradiation;

Reference yield:

: 156150-67-3
3-chloro-4-fluoroiodobenzene

: 1187324-84-0
1-(3-chloro-4-fluorophenyl)-N-(3-chlorophenyl)-5-methyl-1H-1,2,3-triazole-4-carbothiamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium azide / copper(ll) sulfate pentahydrate; sodium carbonate; sodium L-ascorbate; L-proline / water; dimethyl sulfoxide / 20 - 65 °C

2.1: trimethylaluminum / 1,4-dioxane / 20 °C / Inert atmosphere

2.2: 22 h / 20 - 100 °C / Inert atmosphere

2.3: 0.17 h / 20 °C

3.1: Lawessons reagent / toluene / 120 °C / Microwave irradiation

With Lawessons reagent; sodium azide; trimethylaluminum; copper(ll) sulfate pentahydrate; sodium carbonate; sodium L-ascorbate; L-proline; In 1,4-dioxane; water; dimethyl sulfoxide; toluene;

Reference yield:

: 85862-85-7
4-azido-2-chloro-1-fluorobenzene

: 1187324-84-0
1-(3-chloro-4-fluorophenyl)-N-(3-chlorophenyl)-5-methyl-1H-1,2,3-triazole-4-carbothiamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: toluene / 48 h / 120 °C

2.1: trimethylaluminum / 1,4-dioxane / 20 °C / Inert atmosphere

2.2: 22 h / 20 - 100 °C / Inert atmosphere

2.3: 0.17 h / 20 °C

3.1: Lawessons reagent / toluene / 120 °C / Microwave irradiation

With Lawessons reagent; trimethylaluminum; In 1,4-dioxane; toluene;