Technology Process of C7H12O4
There total 6 articles about C7H12O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
water; sodium hydroxide;
In
tetrahydrofuran; methanol;
at 20 ℃;
for 16h;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: dmap; 1H-imidazole / N,N-dimethyl-formamide / 3 h / 0 - 20 °C / Inert atmosphere
2: triethylamine / dichloromethane / 2 h / 20 °C / Inert atmosphere
3: tri-n-butyl-tin hydride; 2,2'-azobis(isobutyronitrile) / toluene / 3 h / Inert atmosphere; Reflux
4: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere
5: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 16 h / 0 - 20 °C / Inert atmosphere
6: water; sodium hydroxide / tetrahydrofuran; methanol / 16 h / 20 °C
With
1H-imidazole; dmap; 2,2'-azobis(isobutyronitrile); di-isopropyl azodicarboxylate; tetrabutyl ammonium fluoride; water; tri-n-butyl-tin hydride; triethylamine; triphenylphosphine; sodium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; toluene;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: triethylamine / dichloromethane / 2 h / 20 °C / Inert atmosphere
2: tri-n-butyl-tin hydride; 2,2'-azobis(isobutyronitrile) / toluene / 3 h / Inert atmosphere; Reflux
3: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere
4: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 16 h / 0 - 20 °C / Inert atmosphere
5: water; sodium hydroxide / tetrahydrofuran; methanol / 16 h / 20 °C
With
2,2'-azobis(isobutyronitrile); di-isopropyl azodicarboxylate; tetrabutyl ammonium fluoride; water; tri-n-butyl-tin hydride; triethylamine; triphenylphosphine; sodium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane; toluene;