2,4-bis(2',2',6',6'-tetramethylpiperidino)-1,3,2,4-diphosphadiborabicyclo{1.1.0}-butan-bis(tetracarbonyleisen)

Base Information

Chemical Name:2,4-bis(2',2',6',6'-tetramethylpiperidino)-1,3,2,4-diphosphadiborabicyclo{1.1.0}-butan-bis(tetracarbonyleisen)
CAS No.:122575-20-6
Molecular Formula:C₂₆H₃₆B₂Fe₂N₂O₈P₂
Molecular Weight:699.844
Hs Code.:

Synonyms:2,4-bis(2',2',6',6'-tetramethylpiperidino)-1,3,2,4-diphosphadiborabicyclo{1.1.0}-butan-bis(tetracarbonyleisen)

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Chemical Property of 2,4-bis(2',2',6',6'-tetramethylpiperidino)-1,3,2,4-diphosphadiborabicyclo{1.1.0}-butan-bis(tetracarbonyleisen)

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Technology Process of 2,4-bis(2',2',6',6'-tetramethylpiperidino)-1,3,2,4-diphosphadiborabicyclo{1.1.0}-butan-bis(tetracarbonyleisen)

There total 2 articles about 2,4-bis(2',2',6',6'-tetramethylpiperidino)-1,3,2,4-diphosphadiborabicyclo{1.1.0}-butan-bis(tetracarbonyleisen) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 122501-48-8
3,4-bis(2',2,'6',6'-tetramethylpiperidino)-1,2-diphospha-3,4-dibora[1.1.0]bicyclobutane

: 15321-51-4
diiron nonacarbonyl

: 13463-40-6,37220-42-1
iron pentacarbonyl

: 122575-20-6
2,4-bis(2',2',6',6'-tetramethylpiperidino)-1,3,2,4-diphosphadiborabicyclo{1.1.0}-butan-bis(tetracarbonyleisen)

Guidance literature:: In toluene; stirring at room temp. under N2 for 1 day; evapn. (vac.) and recrystn. from Et2O; elem. anal.;

Reference yield: 42.0%

: 122501-48-8
3,4-bis(2',2,'6',6'-tetramethylpiperidino)-1,2-diphospha-3,4-dibora[1.1.0]bicyclobutane

: 15321-51-4
diiron nonacarbonyl

: 13463-40-6,37220-42-1
iron pentacarbonyl

: 122575-20-6
2,4-bis(2',2',6',6'-tetramethylpiperidino)-1,3,2,4-diphosphadiborabicyclo{1.1.0}-butan-bis(tetracarbonyleisen)

: 122575-19-3
2,4-bis(2',2',6',6'-tetramethylpiperidino)-1,3,2,4-diphosphadiborabicyclo{1.1.0}butan-tetracarbonyleisen

Guidance literature:: In benzene; stirring for 15 h under N2; distn. (vac), extn. with pentane, insoluble residue was dissolved in CH2Cl2, cooled to -78°C, crystn. of (C5H6N(CH3)4BP(Fe(CO)4)2; pentane extract was also cooled to -78°C to give ((C5H6N(CH3)4BP)2Fe(CO)4); elem. anal.;