1,6-di-O-benzyl-4-O-[3,4,6-tri-O-acetyl-2-deoxy-2-(2,2,2-trichloro-ethoxycarbonylamino)-α-D-glucopyranosyl]-3-O-(2,2,2-trichloro-ethoxycarbonyl)-2-deoxy-2-(2,2,2-trichloro-ethoxy-carbonylamino)-α-D-glucopyranoside

Base Information

Chemical Name:1,6-di-O-benzyl-4-O-[3,4,6-tri-O-acetyl-2-deoxy-2-(2,2,2-trichloro-ethoxycarbonylamino)-α-D-glucopyranosyl]-3-O-(2,2,2-trichloro-ethoxycarbonyl)-2-deoxy-2-(2,2,2-trichloro-ethoxy-carbonylamino)-α-D-glucopyranoside
CAS No.:1372616-72-2
Molecular Formula:C₄₁H₄₅Cl₉N₂O₁₈
Molecular Weight:1172.89
Hs Code.:

1,6-di-O-benzyl-4-O-[3,4,6-tri-O-acetyl-2-deoxy-2-(2,2,2-trichloro-ethoxycarbonylamino)-α-D-glucopyranosyl]-3-O-(2,2,2-trichloro-ethoxycarbonyl)-2-deoxy-2-(2,2,2-trichloro-ethoxy-carbonylamino)-α-D-glucopyranoside

Synonyms:1,6-di-O-benzyl-4-O-[3,4,6-tri-O-acetyl-2-deoxy-2-(2,2,2-trichloro-ethoxycarbonylamino)-α-D-glucopyranosyl]-3-O-(2,2,2-trichloro-ethoxycarbonyl)-2-deoxy-2-(2,2,2-trichloro-ethoxy-carbonylamino)-α-D-glucopyranoside

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Chemical Property of 1,6-di-O-benzyl-4-O-[3,4,6-tri-O-acetyl-2-deoxy-2-(2,2,2-trichloro-ethoxycarbonylamino)-α-D-glucopyranosyl]-3-O-(2,2,2-trichloro-ethoxycarbonyl)-2-deoxy-2-(2,2,2-trichloro-ethoxy-carbonylamino)-α-D-glucopyranoside

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Technology Process of 1,6-di-O-benzyl-4-O-[3,4,6-tri-O-acetyl-2-deoxy-2-(2,2,2-trichloro-ethoxycarbonylamino)-α-D-glucopyranosyl]-3-O-(2,2,2-trichloro-ethoxycarbonyl)-2-deoxy-2-(2,2,2-trichloro-ethoxy-carbonylamino)-α-D-glucopyranoside

There total 9 articles about 1,6-di-O-benzyl-4-O-[3,4,6-tri-O-acetyl-2-deoxy-2-(2,2,2-trichloro-ethoxycarbonylamino)-α-D-glucopyranosyl]-3-O-(2,2,2-trichloro-ethoxycarbonyl)-2-deoxy-2-(2,2,2-trichloro-ethoxy-carbonylamino)-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 1372616-71-1
1,6-di-O-benzyl-2-deoxy-3-O-(2,2,2-trichloro-ethoxycarbonyl)-2-(2,2,2-trichloro-ethoxy-carbonylamino)-α-D-glucopyranoside

: 3,4,6-tri-O-acetyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-D-glucopyranosyl trichloroacetimidate

: 1372616-72-2
1,6-di-O-benzyl-4-O-[3,4,6-tri-O-acetyl-2-deoxy-2-(2,2,2-trichloro-ethoxycarbonylamino)-α-D-glucopyranosyl]-3-O-(2,2,2-trichloro-ethoxycarbonyl)-2-deoxy-2-(2,2,2-trichloro-ethoxy-carbonylamino)-α-D-glucopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -15 ℃; for 0.333333h; Molecular sieve;

Reference yield:

: 339316-68-6
benzyl 2-deoxy-2-(2,2,2-trichloro-ethoxycarbonylamino)-α-D-glucopyranoside

: 1372616-72-2
1,6-di-O-benzyl-4-O-[3,4,6-tri-O-acetyl-2-deoxy-2-(2,2,2-trichloro-ethoxycarbonylamino)-α-D-glucopyranosyl]-3-O-(2,2,2-trichloro-ethoxycarbonyl)-2-deoxy-2-(2,2,2-trichloro-ethoxy-carbonylamino)-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: CSA / acetonitrile / 24 h / 20 °C

2: pyridine / 12 h / 0 - 20 °C

3: triethylsilane; boron trifluoride diethyl etherate / dichloromethane / 3 h / 20 °C

4: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 0.33 h / -15 °C / Molecular sieve

With pyridine; triethylsilane; trimethylsilyl trifluoromethanesulfonate; boron trifluoride diethyl etherate; In dichloromethane; acetonitrile;

Reference yield:

: 1372616-70-0
benzyl 2-deoxy-4,6-O-benzylidene-3-O-(2,2,2-trichloro-ethoxycarbonyl)-2-(2,2,2-trichloro-ethoxycarbonylamino)-α-D-glucopyranoside

: 1372616-72-2
1,6-di-O-benzyl-4-O-[3,4,6-tri-O-acetyl-2-deoxy-2-(2,2,2-trichloro-ethoxycarbonylamino)-α-D-glucopyranosyl]-3-O-(2,2,2-trichloro-ethoxycarbonyl)-2-deoxy-2-(2,2,2-trichloro-ethoxy-carbonylamino)-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: triethylsilane; boron trifluoride diethyl etherate / dichloromethane / 3 h / 20 °C

2: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 0.33 h / -15 °C / Molecular sieve

With triethylsilane; trimethylsilyl trifluoromethanesulfonate; boron trifluoride diethyl etherate; In dichloromethane;