1-(3-methyl-3-hydroxy-1-butynyl)-4-[1-iodo-2,5-di(dodecyloxy)benzene-4-ylethynyl]-2,5-didodecyloxybenzene

Base Information

Chemical Name:1-(3-methyl-3-hydroxy-1-butynyl)-4-[1-iodo-2,5-di(dodecyloxy)benzene-4-ylethynyl]-2,5-didodecyloxybenzene
CAS No.:1353054-14-4
Molecular Formula:C₆₇H₁₁₁IO₅
Molecular Weight:1123.52
Hs Code.:

Synonyms:1-(3-methyl-3-hydroxy-1-butynyl)-4-[1-iodo-2,5-di(dodecyloxy)benzene-4-ylethynyl]-2,5-didodecyloxybenzene

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Chemical Property of 1-(3-methyl-3-hydroxy-1-butynyl)-4-[1-iodo-2,5-di(dodecyloxy)benzene-4-ylethynyl]-2,5-didodecyloxybenzene

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Technology Process of 1-(3-methyl-3-hydroxy-1-butynyl)-4-[1-iodo-2,5-di(dodecyloxy)benzene-4-ylethynyl]-2,5-didodecyloxybenzene

There total 2 articles about 1-(3-methyl-3-hydroxy-1-butynyl)-4-[1-iodo-2,5-di(dodecyloxy)benzene-4-ylethynyl]-2,5-didodecyloxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 243835-38-3
1-(3-hydroxy-3-methyl-1-butynyl)-4-ethynyl-2,5-di(dodecyloxy)benzene

: 145483-66-5
1,4-bis(dodecyloxy)-2,5-diiodobenzene

: 1353054-14-4
1-(3-methyl-3-hydroxy-1-butynyl)-4-[1-iodo-2,5-di(dodecyloxy)benzene-4-ylethynyl]-2,5-didodecyloxybenzene

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In tetrahydrofuran; at 60 ℃; for 12h; Inert atmosphere; Enzymatic reaction;
DOI:10.1002/chem.201100454

Reference yield:

: 145483-66-5
1,4-bis(dodecyloxy)-2,5-diiodobenzene

: 1353054-14-4
1-(3-methyl-3-hydroxy-1-butynyl)-4-[1-iodo-2,5-di(dodecyloxy)benzene-4-ylethynyl]-2,5-didodecyloxybenzene

Guidance literature:: Multi-step reaction with 3 steps

1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / tetrahydrofuran / 12 h / 60 °C / Inert atmosphere

2: sodium hydroxide / toluene / 75 °C

3: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / tetrahydrofuran / 12 h / 60 °C / Inert atmosphere; Enzymatic reaction

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; sodium hydroxide; In tetrahydrofuran; toluene; 1: Sonogashira coupling / 3: Sonogashira coupling;
DOI:10.1002/chem.201100454

Reference yield: 81.0%

: 1353054-14-4
1-(3-methyl-3-hydroxy-1-butynyl)-4-[1-iodo-2,5-di(dodecyloxy)benzene-4-ylethynyl]-2,5-didodecyloxybenzene

: 152270-00-3
1,4-bis(dodecyloxy)-2,5-diethynylbenzene

: 1353054-16-6
C₁₆₈H₂₇₄O₁₂

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In tetrahydrofuran; at 60 ℃; for 12h; Inert atmosphere;
DOI:10.1002/chem.201100454