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C15H20O3

Base Information
  • Chemical Name:C15H20O3
  • CAS No.:1195988-15-8
  • Molecular Formula:C15H20O3
  • Molecular Weight:248.322
  • Hs Code.:
C<sub>15</sub>H<sub>20</sub>O<sub>3</sub>

Synonyms:C15H20O3

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Chemical Property of C15H20O3
Chemical Property:
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Technology Process of C15H20O3

There total 1 articles about C15H20O3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 - 20 ℃; for 13h;
DOI:10.1016/j.tet.2010.11.017
Guidance literature:
C15H20O3; With titanium(IV) isopropylate; diethyl (2R,3R)-tartrate; Cumene hydroperoxide; In dichloromethane; at -40 - -25 ℃; for 9h; Molecular sieve;
With tributylphosphine; citric acid; In dichloromethane; water; acetone; at -25 - 20 ℃; for 1.5h;
DOI:10.1016/j.tet.2010.11.017
Guidance literature:
Multi-step reaction with 5 steps
1.1: titanium(IV) isopropylate; diethyl (2R,3R)-tartrate; Cumene hydroperoxide / dichloromethane / 9 h / -40 - -25 °C / Molecular sieve
1.2: 1.5 h / -25 - 20 °C
2.1: di(n-butyl)tin oxide; triethylamine / dichloromethane / 13.83 h / 20 °C
3.1: potassium carbonate / methanol / 4 h / 20 °C
4.1: copper(l) iodide / tetrahydrofuran / 1.5 h / -40 °C
5.1: dmap; triethylamine / 2.5 h / 20 °C
With titanium(IV) isopropylate; dmap; copper(l) iodide; diethyl (2R,3R)-tartrate; Cumene hydroperoxide; di(n-butyl)tin oxide; potassium carbonate; triethylamine; In tetrahydrofuran; methanol; dichloromethane; 1.1: Sharpless epoxidation;
DOI:10.1016/j.tet.2010.11.017
upstream raw materials:

C21H34O3Si

Downstream raw materials:

C15H20O4

C20H26O4

C32H48O6Si

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