12-di-n-butylphosphonododecan-1-ol trityl ether

Base Information

Chemical Name:12-di-n-butylphosphonododecan-1-ol trityl ether
CAS No.:307315-52-2
Molecular Formula:C₃₉H₅₇O₄P
Molecular Weight:620.853
Hs Code.:

Synonyms:12-di-n-butylphosphonododecan-1-ol trityl ether

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Chemical Property of 12-di-n-butylphosphonododecan-1-ol trityl ether

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Technology Process of 12-di-n-butylphosphonododecan-1-ol trityl ether

There total 3 articles about 12-di-n-butylphosphonododecan-1-ol trityl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1809-19-4
dibutyl hydrogen phosphite

: 307315-51-1
12-iodododecan-1-ol trityl ether

: 307315-52-2
12-di-n-butylphosphonododecan-1-ol trityl ether

Guidance literature:: With sodium; In hexane; Heating;
DOI:10.1016/S0040-4020(00)00546-9

Reference yield:

: 71736-19-1
12-iodododecan-1-oic acid

: 307315-52-2
12-di-n-butylphosphonododecan-1-ol trityl ether

Guidance literature:: Multi-step reaction with 3 steps

1: 77 percent / sodium borohydride; TiCl₄ / 1,2-dimethoxy-ethane / 0 - 20 °C

2: 90 percent / tetraethylammonium perchlorate; 2,4,6-collidine / CH₂Cl₂ / 0.5 h

3: 92 percent / sodium / hexane / Heating

With 2,4,6-trimethyl-pyridine; sodium tetrahydroborate; tetraethylammonium perchlorate; sodium; titanium tetrachloride; In 1,2-dimethoxyethane; hexane; dichloromethane; 3: Michaelis-Becker reaction;
DOI:10.1016/S0040-4020(00)00546-9

Reference yield:

: 57395-52-5
12-iodo-1-dodecanol

: 307315-52-2
12-di-n-butylphosphonododecan-1-ol trityl ether

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / tetraethylammonium perchlorate; 2,4,6-collidine / CH₂Cl₂ / 0.5 h

2: 92 percent / sodium / hexane / Heating

With 2,4,6-trimethyl-pyridine; tetraethylammonium perchlorate; sodium; In hexane; dichloromethane; 2: Michaelis-Becker reaction;
DOI:10.1016/S0040-4020(00)00546-9