C₄₆H₅₄N₂O₁₀Si

Base Information

Chemical Name:C₄₆H₅₄N₂O₁₀Si
CAS No.:1359022-13-1
Molecular Formula:C₄₆H₅₄N₂O₁₀Si
Molecular Weight:823.028
Hs Code.:

C<sub>46</sub>H<sub>54</sub>N<sub>2</sub>O<sub>10</sub>Si

Synonyms:C₄₆H₅₄N₂O₁₀Si

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Chemical Property of C₄₆H₅₄N₂O₁₀Si

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Technology Process of C₄₆H₅₄N₂O₁₀Si

There total 13 articles about C₄₆H₅₄N₂O₁₀Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 852821-06-8
(4aS,8aS,9S)-3-(benzyloxy)-4a-(tert-butyldimethylsilyloxy)-9-(dimethylamino)-8a,9-dihydronaphtho[2,3-d]isoxazole-4,5(4aH,8H)-dione

: 1359022-12-0
C₂₆H₂₆O₆

: 1359022-13-1
C₄₆H₅₄N₂O₁₀Si

Guidance literature:: C₂₆H₂₆O₆; With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; diisopropylamine; In tetrahydrofuran; at -78 ℃; for 0.5h;

(4aS,8aS,9S)-3-(benzyloxy)-4a-(tert-butyldimethylsilyloxy)-9-(dimethylamino)-8a,9-dihydronaphtho[2,3-d]isoxazole-4,5(4aH,8H)-dione; In tetrahydrofuran; at -100 - -20 ℃; for 1h;

With ammonium chloride; In tetrahydrofuran; water; ethyl acetate;

Reference yield:

: 50868-73-0
2-methoxy-6-methylbenzeneamine

: 1359022-13-1
C₄₆H₅₄N₂O₁₀Si

Guidance literature:: Multi-step reaction with 13 steps

1.1: bromine; acetic acid / methanol / 2 h / 20 °C / Cooling with ice

2.1: hydrogenchloride; sodium nitrite / water / 0.5 h / 0 °C

2.2: 4 h / 0 - 50 °C

3.1: diisobutylaluminium hydride / tetrahydrofuran; toluene / -78 - 20 °C

3.2: 1 h / 20 °C

4.1: sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 0.5 h / 20 °C

4.2: pH 1

5.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 0.5 h / 20 °C

6.1: triethylamine / dmap / 1 h / 20 °C

7.1: boron tribromide / dichloromethane / 0.58 h / -78 - 0 °C

7.2: 0.33 h / 20 °C

8.1: [bis(acetoxy)iodo]benzene / 1,4-dioxane / 17 h / 0 - 20 °C

8.2: 0.33 h / 20 °C

9.1: potassium carbonate / acetone / 2 h / Reflux

10.1: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 90 °C / Inert atmosphere

11.1: hydrogen / 30 wt % Pd/C / methanol / 1 h / 20 °C

12.1: dmap / dichloromethane / 1.5 h / 20 °C

13.1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine; diisopropylamine / tetrahydrofuran / 0.5 h / -78 °C

13.2: 1 h / -100 - -20 °C

With hydrogenchloride; sodium chlorite; sodium dihydrogenphosphate; n-butyllithium; 2-methyl-but-2-ene; oxalyl dichloride; N,N,N,N,-tetramethylethylenediamine; [bis(acetoxy)iodo]benzene; hydrogen; bromine; boron tribromide; diisobutylaluminium hydride; potassium carbonate; acetic acid; triethylamine; diisopropylamine; sodium nitrite; dmap; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 30 wt % Pd/C; N,N-dimethyl-formamide; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; acetone; toluene; tert-butyl alcohol;

Reference yield:

: 877149-05-8
4-bromo-2-methoxy-6-methyl-benzonitrile

: 1359022-13-1
C₄₆H₅₄N₂O₁₀Si

Guidance literature:: Multi-step reaction with 11 steps

1.1: diisobutylaluminium hydride / tetrahydrofuran; toluene / -78 - 20 °C

1.2: 1 h / 20 °C

2.1: sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 0.5 h / 20 °C

2.2: pH 1

3.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 0.5 h / 20 °C

4.1: triethylamine / dmap / 1 h / 20 °C

5.1: boron tribromide / dichloromethane / 0.58 h / -78 - 0 °C

5.2: 0.33 h / 20 °C

6.1: [bis(acetoxy)iodo]benzene / 1,4-dioxane / 17 h / 0 - 20 °C

6.2: 0.33 h / 20 °C

7.1: potassium carbonate / acetone / 2 h / Reflux

8.1: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 90 °C / Inert atmosphere

9.1: hydrogen / 30 wt % Pd/C / methanol / 1 h / 20 °C

10.1: dmap / dichloromethane / 1.5 h / 20 °C

11.1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine; diisopropylamine / tetrahydrofuran / 0.5 h / -78 °C

11.2: 1 h / -100 - -20 °C

With sodium chlorite; sodium dihydrogenphosphate; n-butyllithium; 2-methyl-but-2-ene; oxalyl dichloride; N,N,N,N,-tetramethylethylenediamine; [bis(acetoxy)iodo]benzene; hydrogen; boron tribromide; diisobutylaluminium hydride; potassium carbonate; triethylamine; diisopropylamine; dmap; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 30 wt % Pd/C; N,N-dimethyl-formamide; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; acetone; toluene; tert-butyl alcohol;