N-allyl-N-diphenylphosphinoyl-2-amino-3-phenoxypropyl phenyl selenide

Base Information

Chemical Name:N-allyl-N-diphenylphosphinoyl-2-amino-3-phenoxypropyl phenyl selenide
CAS No.:281669-98-5
Molecular Formula:C₃₀H₃₀NO₂PSe
Molecular Weight:546.507
Hs Code.:

Synonyms:N-allyl-N-diphenylphosphinoyl-2-amino-3-phenoxypropyl phenyl selenide

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Chemical Property of N-allyl-N-diphenylphosphinoyl-2-amino-3-phenoxypropyl phenyl selenide

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Technology Process of N-allyl-N-diphenylphosphinoyl-2-amino-3-phenoxypropyl phenyl selenide

There total 4 articles about N-allyl-N-diphenylphosphinoyl-2-amino-3-phenoxypropyl phenyl selenide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 281669-89-4
N-allyl-2-amino-3-phenoxypropyl phenyl selenide

: 1499-21-4
Diphenylphosphinic chloride

: 281669-98-5
N-allyl-N-diphenylphosphinoyl-2-amino-3-phenoxypropyl phenyl selenide

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 20 ℃;
DOI:10.1021/ol005829x

Reference yield:

: 1666-13-3
diphenyl diselenide

: 281669-98-5
N-allyl-N-diphenylphosphinoyl-2-amino-3-phenoxypropyl phenyl selenide

Guidance literature:: Multi-step reaction with 2 steps

1.1: NaBH₄ / tetrahydrofuran

1.2: 83 percent / TFA

2.1: 82 percent / Et₃N; DMAP / CH₂Cl₂ / 20 °C

With dmap; sodium tetrahydroborate; triethylamine; In tetrahydrofuran; dichloromethane; 1.1: Reduction / 1.2: Ring cleavage / 2.1: Substitution;
DOI:10.1021/ol005829x

Reference yield:

: 281669-86-1
N-allyl-2-phenoxymethyl-aziridine

: 281669-98-5
N-allyl-N-diphenylphosphinoyl-2-amino-3-phenoxypropyl phenyl selenide

Guidance literature:: Multi-step reaction with 2 steps

1.1: NaBH₄ / tetrahydrofuran

1.2: 83 percent / TFA

2.1: 82 percent / Et₃N; DMAP / CH₂Cl₂ / 20 °C

With dmap; sodium tetrahydroborate; triethylamine; In tetrahydrofuran; dichloromethane; 1.1: Reduction / 1.2: Ring cleavage / 2.1: Substitution;
DOI:10.1021/ol005829x