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Technology Process of 1-((1R,2S,3S,5S,6R,7S)-5-Methyl-4,4-dioxo-4λ6-thia-tricyclo[5.2.1.02,6]dec-8-en-3-yl)-cyclohexanol

1-((1R,2S,3S,5S,6R,7S)-5-Methyl-4,4-dioxo-4λ6-thia-tricyclo[5.2.1.02,6]dec-8-en-3-yl)-cyclohexanol

Base Information
  • Chemical Name:1-((1R,2S,3S,5S,6R,7S)-5-Methyl-4,4-dioxo-4λ6-thia-tricyclo[5.2.1.02,6]dec-8-en-3-yl)-cyclohexanol
  • CAS No.:88920-66-5
  • Molecular Formula:C16H24O3S
  • Molecular Weight:296.431
  • Hs Code.:
1-((1R,2S,3S,5S,6R,7S)-5-Methyl-4,4-dioxo-4λ<sup>6</sup>-thia-tricyclo[5.2.1.0<sup>2,6</sup>]dec-8-en-3-yl)-cyclohexanol

Synonyms:1-((1R,2S,3S,5S,6R,7S)-5-Methyl-4,4-dioxo-4λ6-thia-tricyclo[5.2.1.02,6]dec-8-en-3-yl)-cyclohexanol

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Chemical Property of 1-((1R,2S,3S,5S,6R,7S)-5-Methyl-4,4-dioxo-4λ6-thia-tricyclo[5.2.1.02,6]dec-8-en-3-yl)-cyclohexanol
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Technology Process of 1-((1R,2S,3S,5S,6R,7S)-5-Methyl-4,4-dioxo-4λ6-thia-tricyclo[5.2.1.02,6]dec-8-en-3-yl)-cyclohexanol

There total 1 articles about 1-((1R,2S,3S,5S,6R,7S)-5-Methyl-4,4-dioxo-4λ6-thia-tricyclo[5.2.1.02,6]dec-8-en-3-yl)-cyclohexanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

cyclohexanone
108-94-1,11119-77-0,9003-41-2,9075-99-4

cyclohexanone

(1S,2R,3S,6S,7R)-3-Methyl-4-thia-tricyclo[5.2.1.0<sup>2,6</sup>]dec-8-ene 4,4-dioxide
83927-50-8,88979-80-0

(1S,2R,3S,6S,7R)-3-Methyl-4-thia-tricyclo[5.2.1.02,6]dec-8-ene 4,4-dioxide

1-((1R,2S,3S,5S,6R,7S)-5-Methyl-4,4-dioxo-4λ<sup>6</sup>-thia-tricyclo[5.2.1.0<sup>2,6</sup>]dec-8-en-3-yl)-cyclohexanol
88920-66-5

1-((1R,2S,3S,5S,6R,7S)-5-Methyl-4,4-dioxo-4λ6-thia-tricyclo[5.2.1.02,6]dec-8-en-3-yl)-cyclohexanol

Guidance literature:
With n-butyllithium; In tetrahydrofuran; at -78 ℃;
DOI:10.1016/S0040-4039(00)86229-2
upstream raw materials:

cyclohexanone

(1S,2R,3S,6S,7R)-3-Methyl-4-thia-tricyclo[5.2.1.02,6]dec-8-ene 4,4-dioxide

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