methyl 3-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-2,4-dideoxy-4-C-<(methoxycarbonyl)methyl>-α-D-ribo-hexopyranoside

Base Information

Chemical Name:methyl 3-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-2,4-dideoxy-4-C-<(methoxycarbonyl)methyl>-α-D-ribo-hexopyranoside
CAS No.:65011-71-4
Molecular Formula:C₃₃H₄₀O₇Si
Molecular Weight:576.762
Hs Code.:

Synonyms:methyl 3-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-2,4-dideoxy-4-C-<(methoxycarbonyl)methyl>-α-D-ribo-hexopyranoside

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Chemical Property of methyl 3-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-2,4-dideoxy-4-C-<(methoxycarbonyl)methyl>-α-D-ribo-hexopyranoside

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Technology Process of methyl 3-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-2,4-dideoxy-4-C-<(methoxycarbonyl)methyl>-α-D-ribo-hexopyranoside

There total 10 articles about methyl 3-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-2,4-dideoxy-4-C-<(methoxycarbonyl)methyl>-α-D-ribo-hexopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 65011-70-3
methyl 3-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-2,4-dideoxy-4-C--α-D-erythro-hexopyranoside

: 65011-71-4
methyl 3-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-2,4-dideoxy-4-C-<(methoxycarbonyl)methyl>-α-D-ribo-hexopyranoside

Guidance literature:: With hydrogen; palladium hydroxide - carbon; In methanol; ethyl acetate; for 24h;
DOI:10.1139/v81-126

Reference yield: 70.0%

: 65011-69-0,65011-70-3
methyl 3-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-2,4-dideoxy-4-C--α-D-erythro-hexopyranoside

: 65011-71-4
methyl 3-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-2,4-dideoxy-4-C-<(methoxycarbonyl)methyl>-α-D-ribo-hexopyranoside

Guidance literature:: With hydrogen; palladium hydroxide - carbon; In methanol; ethyl acetate; for 24h;
DOI:10.1139/v81-126

Reference yield:

: 65011-68-9
methyl 3-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-2-deoxy-α-D-erythro-hexopyranosid-4-ulose

: 65011-71-4
methyl 3-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-2,4-dideoxy-4-C-<(methoxycarbonyl)methyl>-α-D-ribo-hexopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 48.6 percent / potassium tert-butoxide / toluene / 8 h / Ambient temperature

2: 92 percent / H₂ / 20percent palladium hydroxide on charcoal / methanol; ethyl acetate / 24 h

With potassium tert-butylate; hydrogen; palladium hydroxide - carbon; In methanol; ethyl acetate; toluene;
DOI:10.1139/v81-126