(2R,3S,4R,5R,6R)-2-(acetoxymethyl)-6-(cyclohexylthio)-5-((E)-4-phenylbut-1-enylsulfonamido)-tetrahydro-2H-pyran-3,4-diyl diacetate

Base Information

• Chemical Name: (2R,3S,4R,5R,6R)-2-(acetoxymethyl)-6-(cyclohexylthio)-5-((E)-4-phenylbut-1-enylsulfonamido)-tetrahydro-2H-pyran-3,4-diyl diacetate
• CAS No.: 1002105-79-4
• Molecular Formula: C₂₈H₃₉NO₉S₂
• Molecular Weight: 597.751

Synonyms:(2R,3S,4R,5R,6R)-2-(acetoxymethyl)-6-(cyclohexylthio)-5-((E)-4-phenylbut-1-enylsulfonamido)-tetrahydro-2H-pyran-3,4-diyl diacetate

Chemical Property of (2R,3S,4R,5R,6R)-2-(acetoxymethyl)-6-(cyclohexylthio)-5-((E)-4-phenylbut-1-enylsulfonamido)-tetrahydro-2H-pyran-3,4-diyl diacetate

Chemical Property:

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Technology Process of (2R,3S,4R,5R,6R)-2-(acetoxymethyl)-6-(cyclohexylthio)-5-((E)-4-phenylbut-1-enylsulfonamido)-tetrahydro-2H-pyran-3,4-diyl diacetate

There total 1 articles about (2R,3S,4R,5R,6R)-2-(acetoxymethyl)-6-(cyclohexylthio)-5-((E)-4-phenylbut-1-enylsulfonamido)-tetrahydro-2H-pyran-3,4-diyl diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

4-phenyl-but-1E-ene-1-sulfonyl chloride (1002105-78-3) + (2R,3S,4R,5R,6R)-2-(acetoxymethyl)-5-amino-6-(cyclohexylthio)-tetrahydro-2H-pyran-3,4-diyl diacetate (1002105-43-2) → (2R,3S,4R,5R,6R)-2-(acetoxymethyl)-6-(cyclohexylthio)-5-((E)-4-phenylbut-1-enylsulfonamido)-tetrahydro-2H-pyran-3,4-diyl diacetate (1002105-79-4)

Guidance literature:

With triethylamine; In dichloromethane; at 20 ℃; for 4h;

DOI:10.1021/jm070669h

Reference yield: 91.0%

(2R,3S,4R,5R,6R)-2-(acetoxymethyl)-6-(cyclohexylthio)-5-((E)-4-phenylbut-1-enylsulfonamido)-tetrahydro-2H-pyran-3,4-diyl diacetate (1002105-79-4) → (E)-N-((2R,3R,4R,5S,6R)-2-(cyclohexylthio)-4,5-dihydroxy-6-(hydroxymethyl)-tetrahydro-2H-pyran-3-yl)-4-phenylbut-1-ene-1-sulfonamide (1002105-50-1)

Guidance literature:

With sodium methylate; In methanol; at 20 ℃;

DOI:10.1021/jm070669h

Reference yield:

(2R,3S,4R,5R,6R)-2-(acetoxymethyl)-6-(cyclohexylthio)-5-((E)-4-phenylbut-1-enylsulfonamido)-tetrahydro-2H-pyran-3,4-diyl diacetate (1002105-79-4) → N-((2R,3R,4R,5S,6R)-2-(cyclohexylthio)-4,5-dihydroxy-6-(hydroxymethyl)-tetrahydro-2H-pyran-3-yl)-4-phenylbutane-1-sulfonamide (1002105-52-3)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethanol; for 8h; under 760.051 Torr;

DOI:10.1021/jm070669h

upstream raw materials:

4-phenyl-but-1E-ene-1-sulfonyl chloride

(2R,3S,4R,5R,6R)-2-(acetoxymethyl)-5-amino-6-(cyclohexylthio)-tetrahydro-2H-pyran-3,4-diyl diacetate

Downstream raw materials:

(E)-N-((2R,3R,4R,5S,6R)-2-(cyclohexylthio)-4,5-dihydroxy-6-(hydroxymethyl)-tetrahydro-2H-pyran-3-yl)-4-phenylbut-1-ene-1-sulfonamide

N-((2R,3R,4R,5S,6R)-2-(cyclohexylthio)-4,5-dihydroxy-6-(hydroxymethyl)-tetrahydro-2H-pyran-3-yl)-4-phenylbutane-1-sulfonamide

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