2-(5-tert-butyl-2-ethyl-2H-pyrazol-3-yl)-7-methyl-5-(2-trifluoromethylphenyl)-1H-benzimidazole

Base Information

Chemical Name:2-(5-tert-butyl-2-ethyl-2H-pyrazol-3-yl)-7-methyl-5-(2-trifluoromethylphenyl)-1H-benzimidazole
CAS No.:1392516-99-2
Molecular Formula:C₂₄H₂₅F₃N₄
Molecular Weight:426.485
Hs Code.:

Synonyms:2-(5-tert-butyl-2-ethyl-2H-pyrazol-3-yl)-7-methyl-5-(2-trifluoromethylphenyl)-1H-benzimidazole

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Chemical Property of 2-(5-tert-butyl-2-ethyl-2H-pyrazol-3-yl)-7-methyl-5-(2-trifluoromethylphenyl)-1H-benzimidazole

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Technology Process of 2-(5-tert-butyl-2-ethyl-2H-pyrazol-3-yl)-7-methyl-5-(2-trifluoromethylphenyl)-1H-benzimidazole

There total 2 articles about 2-(5-tert-butyl-2-ethyl-2H-pyrazol-3-yl)-7-methyl-5-(2-trifluoromethylphenyl)-1H-benzimidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 167889-79-4
1-ethyl-3-tert-butyl-4-H-pyrazole chloride

: 1221350-15-7
5-methyl-2'-trifluoromethyl-biphenyl-3,4-diamine

: 1392516-99-2
2-(5-tert-butyl-2-ethyl-2H-pyrazol-3-yl)-7-methyl-5-(2-trifluoromethylphenyl)-1H-benzimidazole

Guidance literature:: 1-ethyl-3-tert-butyl-4-H-pyrazole chloride; 5-methyl-2'-trifluoromethyl-biphenyl-3,4-diamine; With triethylamine; In dichloromethane; at 20 ℃;

With camphor-10-sulfonic acid; In 1,4-dioxane; at 100 ℃; for 3h;

With triethylamine; In 1,4-dioxane; at 20 ℃;

Reference yield:

: 1392516-93-6
3-methyl-5-nitro-2'-trifluoromethyl-biphenyl-4-ylamine

: 1392516-99-2
2-(5-tert-butyl-2-ethyl-2H-pyrazol-3-yl)-7-methyl-5-(2-trifluoromethylphenyl)-1H-benzimidazole

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride; iron / ethanol; water / 4 h / 80 °C

2.1: triethylamine / dichloromethane / 20 °C

2.2: 3 h / 100 °C

2.3: 20 °C

With hydrogenchloride; iron; triethylamine; In ethanol; dichloromethane; water;