2,4-dimethyl-3-phenylquinoline

Base Information

Chemical Name:2,4-dimethyl-3-phenylquinoline
CAS No.:7055-05-2
Molecular Formula:C₁₇H₁₅N
Molecular Weight:233.313
Hs Code.:

Synonyms:2,4-dimethyl-3-phenylquinoline

Suppliers and Price of 2,4-dimethyl-3-phenylquinoline

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Chemical Property of 2,4-dimethyl-3-phenylquinoline

Chemical Property:

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Technology Process of 2,4-dimethyl-3-phenylquinoline

There total 6 articles about 2,4-dimethyl-3-phenylquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 673-32-5
1-Phenylprop-1-yne

: 103-84-4
Acetanilid

: 7055-05-2
2,4-dimethyl-3-phenylquinoline

Guidance literature:: With di-μ-chloro-bis[chloro(η⁵-pentamethylcyclopentadienyl)cobalt]; silver(I) triflimide; In 1,2-dichloro-ethane; at 130 ℃; for 16h; regioselective reaction; Sealed tube;
DOI:10.1021/acs.orglett.5b03629

Reference yield: 62.0%

: 91-55-4
2,3-dimethylindole

: 4460-46-2
3-chloro-3-phenyl-3H-diazirine

: 7055-05-2
2,4-dimethyl-3-phenylquinoline

Guidance literature:: With sodium carbonate; In acetonitrile; at 50 ℃; for 12h; Sealed tube;
DOI:10.1021/jacs.1c06287

Reference yield:

: 1670-14-0
benzamidine monohydrochloride

: 7055-05-2
2,4-dimethyl-3-phenylquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: lithium chloride; sodium chloride; sodium hypochlorite / dimethyl sulfoxide; pentane / 0 °C

2: sodium carbonate / acetonitrile / 12 h / 50 °C / Sealed tube

With sodium hypochlorite; sodium carbonate; lithium chloride; sodium chloride; In dimethyl sulfoxide; acetonitrile; pentane; 2: |Ciamician-Dennstedt Rearrangement;
DOI:10.1021/jacs.1c06287